(Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino-P-borane]ethane

Base Information

Chemical Name:(Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino-P-borane]ethane
CAS No.:917029-50-6
Molecular Formula:C₃₄H₅₀B₂O₂P₂Si₂
Molecular Weight:630.51
Hs Code.:

Synonyms:(Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino-P-borane]ethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino-P-borane]ethane

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Technology Process of (Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino-P-borane]ethane

There total 2 articles about (Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino-P-borane]ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 4206-67-1
iodo(trimethylsilyl)methane

: 1316041-04-9,917029-15-3
(R_P,R_P)-1,2-bis[(o-hydroxyphenyl)(phenyl)phosphino-P-borane]ethane

: 917029-50-6
(Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino-P-borane]ethane

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 40 ℃; Inert atmosphere;
DOI:10.1021/ol100184p

Reference yield:

: 1316041-04-9,917029-15-3
(R_P,R_P)-1,2-bis[(o-hydroxyphenyl)(phenyl)phosphino-P-borane]ethane

: 917029-50-6
(Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino-P-borane]ethane

Guidance literature:: With K₂CO₃; In N,N-dimethyl-formamide; mixt. of B compd., K2CO3 and Me3SiCH2 iodide, bromide or tosylate in DMFstirred at 40°C; concd.; filtered through silica gel pad; eluted with CH2Cl2; recrystd. from hexane-CH2Cl2;
DOI:10.1039/c1ob05364g