(Rp,Rp)-1,2-bis{(phenyl)[2-(trimethylsilylmethoxy)phenyl]phosphino}ethane

Base Information

Chemical Name:(Rp,Rp)-1,2-bis{(phenyl)[2-(trimethylsilylmethoxy)phenyl]phosphino}ethane
CAS No.:917029-72-2
Molecular Formula:C₃₄H₄₄O₂P₂Si₂
Molecular Weight:602.841
Hs Code.:

Synonyms:(Rp,Rp)-1,2-bis{(phenyl)[2-(trimethylsilylmethoxy)phenyl]phosphino}ethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Rp,Rp)-1,2-bis{(phenyl)[2-(trimethylsilylmethoxy)phenyl]phosphino}ethane

Chemical Property:

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Technology Process of (Rp,Rp)-1,2-bis{(phenyl)[2-(trimethylsilylmethoxy)phenyl]phosphino}ethane

There total 2 articles about (Rp,Rp)-1,2-bis{(phenyl)[2-(trimethylsilylmethoxy)phenyl]phosphino}ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 917029-50-6
(Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino-P-borane]ethane

: 917029-72-2
(Rp,Rp)-1,2-bis{(phenyl)[2-(trimethylsilylmethoxy)phenyl]phosphino}ethane

Guidance literature:: In diethylamine; Reflux; Inert atmosphere;
DOI:10.1021/ol100184p

Reference yield:

: 917029-72-2
(Rp,Rp)-1,2-bis{(phenyl)[2-(trimethylsilylmethoxy)phenyl]phosphino}ethane

Guidance literature:

Reference yield:

: di(norbornadiene)rhodium(I) tetrafluoroborate

: 917029-72-2
(Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino]ethane

: [Rh((Rp,Rp)-1,2-bis[(o-(trimethylsilylmethyloxy)phenyl)(phenyl)phosphino]ethane)(MeOH)2]BF₄

: 378784-00-0,7440-16-6
rhodium

Guidance literature:: With H₂; In methanol; soln. of ligand in MeOH added dropwise at room temp. to soln. of Rh complex in MeOH; hydrogenated under H2 (1 bar) for ca. 15 min; soln. filtered; not isolated;
DOI:10.1039/c1ob05364g