Benzo[b]1,4-dioxin-2-ol, 2,3-dihydro-3-benzoyl-

Base Information

Chemical Name:Benzo[b]1,4-dioxin-2-ol, 2,3-dihydro-3-benzoyl-
CAS No.:287933-34-0
Molecular Formula:C₁₅H₁₂O₄
Molecular Weight:256.258
Hs Code.:
DSSTox Substance ID:DTXSID201189095

Synonyms:Enamine_000297;Oprea1_546037;Benzo[b]1,4-dioxin-2-ol, 2,3-dihydro-3-benzoyl-;DTXSID201189095;HMS1394N11;SR-01000025850;SR-01000025850-1;Z56763840;(2,3-Dihydro-3-hydroxy-1,4-benzodioxin-2-yl)phenylmethanone;(3-Hydroxy-2,3-dihydro-1,4-benzodioxin-2-yl)(phenyl)methanone #;287933-34-0

Suppliers and Price of Benzo[b]1,4-dioxin-2-ol, 2,3-dihydro-3-benzoyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzo[b]1,4-dioxin-2-ol, 2,3-dihydro-3-benzoyl-

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:256.07355886
Heavy Atom Count:19
Complexity:324

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)C2C(OC3=CC=CC=C3O2)O

Technology Process of Benzo[b]1,4-dioxin-2-ol, 2,3-dihydro-3-benzoyl-

There total 2 articles about Benzo[b]1,4-dioxin-2-ol, 2,3-dihydro-3-benzoyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 287933-33-9
3-formyl-2-phenyl-1,4-benzodioxine

: 287933-34-0
3-benzoyl-2,3-dihydro-1,4-benzodioxin-2-ol

Guidance literature:: With hydrogenchloride; In water; acetic acid; Heating;
DOI:10.1007/BF02251825

Reference yield:

: 5770-58-1
2-phenylbenzo[b][1,4]dioxine

: 287933-34-0
3-benzoyl-2,3-dihydro-1,4-benzodioxin-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / POCl₃ / 24 h / 20 °C

2: 94 percent / conc. HCl / acetic acid; H₂O / 0.75 h / 95 - 100 °C

With hydrogenchloride; trichlorophosphate; In water; acetic acid; 1: Formylation / 2: hydration;
DOI:10.1007/BF02256876