Technology Process of O-methyl styelsamine-N14-2-phenylacetamide
There total 8 articles about O-methyl styelsamine-N14-2-phenylacetamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
PyBOP; triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.3390/md11020274
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: cerium(III) chloride heptahydrate; silver(l) oxide / acetic acid; methanol / 1.5 h / 40 °C / Inert atmosphere
1.2: 0.5 h / 90 °C
2.1: hydrogenchloride / water / 48 h / 80 °C
3.1: triethylamine; PyBOP / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
With
hydrogenchloride; cerium(III) chloride heptahydrate; PyBOP; triethylamine; silver(l) oxide;
In
methanol; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.3390/md11020274
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydroxide / water; ethyl acetate / 0.5 h / 20 °C / Inert atmosphere
2.1: ozone / Cooling with ice
2.2: 1.5 h / 40 °C
3.1: hydrogen bromide / acetic acid / 18 h / 80 °C / Inert atmosphere
4.1: cerium(III) chloride heptahydrate; silver(l) oxide / acetic acid; methanol / 1.5 h / 40 °C / Inert atmosphere
4.2: 0.5 h / 90 °C
5.1: hydrogenchloride / water / 48 h / 80 °C
6.1: triethylamine; PyBOP / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
With
hydrogenchloride; cerium(III) chloride heptahydrate; PyBOP; hydrogen bromide; ozone; triethylamine; sodium hydroxide; silver(l) oxide;
In
methanol; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.3390/md11020274
