N-phenyl-N-(3-methyl-2-oxo-1-pentyl)triflamide

Base Information

• Chemical Name: N-phenyl-N-(3-methyl-2-oxo-1-pentyl)triflamide
• CAS No.: 71901-58-1
• Molecular Formula: C₁₃H₁₆F₃NO₃S
• Molecular Weight: 323.336
• Mol file: 71901-58-1.mol

Synonyms:N-phenyl-N-(3-methyl-2-oxo-1-pentyl)triflamide

Chemical Property of N-phenyl-N-(3-methyl-2-oxo-1-pentyl)triflamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of N-phenyl-N-(3-methyl-2-oxo-1-pentyl)triflamide

There total 2 articles about N-phenyl-N-(3-methyl-2-oxo-1-pentyl)triflamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.8%

phenyl trifluoromethanesulfonamide (456-64-4) + 1-iodo-3-methyl-2-pentanone (71886-29-8) → N-phenyl-N-(3-methyl-2-oxo-1-pentyl)triflamide (71901-58-1)

Guidance literature:

With potassium carbonate; In acetone; for 6h; Heating;

DOI:10.1021/jo01289a033

Reference yield:

3-methyl-1-pentene (760-20-3,13643-02-2) → N-phenyl-N-(3-methyl-2-oxo-1-pentyl)triflamide (71901-58-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 54.4 percent / Ag₂CrO₄ / CH₂Cl₂

2: 95.8 percent / K₂CO₃ / acetone / 6 h / Heating

With silver(I) chromate; potassium carbonate; In dichloromethane; acetone;

DOI:10.1021/jo01289a033

upstream raw materials:

phenyl trifluoromethanesulfonamide

1-iodo-3-methyl-2-pentanone

3-methyl-1-pentene