3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

Base Information

Chemical Name:3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose
CAS No.:1400908-43-1
Molecular Formula:C₃₃H₄₂O₆Si
Molecular Weight:562.778
Hs Code.:

Synonyms:3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

There total 4 articles about 3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1400908-42-0
5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

: 1400908-43-1
3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

Guidance literature:: With potassium carbonate; In methanol; at 25 ℃; for 0.5h; Inert atmosphere;
DOI:10.1055/s-0031-1289783

Reference yield:

: 843674-28-2
C₁₉H₂₆O₇

: 1400908-43-1
3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3.17 h / 0 - 25 °C / Inert atmosphere

2: 1H-imidazole / dichloromethane / 1 h / 25 °C / Inert atmosphere

3: pyridine / 3 h / 25 °C / Inert atmosphere

4: potassium carbonate / methanol / 0.5 h / 25 °C / Inert atmosphere

With pyridine; 1H-imidazole; lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1055/s-0031-1289783

Reference yield:

: C₁₇H₂₄O₆

: 1400908-43-1
3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / dichloromethane / 1 h / 25 °C / Inert atmosphere

2: pyridine / 3 h / 25 °C / Inert atmosphere

3: potassium carbonate / methanol / 0.5 h / 25 °C / Inert atmosphere

With pyridine; 1H-imidazole; potassium carbonate; In methanol; dichloromethane;
DOI:10.1055/s-0031-1289783