5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

Base Information

Chemical Name:5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose
CAS No.:1400908-42-0
Molecular Formula:C₃₅H₄₄O₇Si
Molecular Weight:604.816
Hs Code.:

Synonyms:5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

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Chemical Property of 5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

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Technology Process of 5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

There total 2 articles about 5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 843674-28-2
C₁₉H₂₆O₇

: 5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

: 1400908-42-0
5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3.17 h / 0 - 25 °C / Inert atmosphere

2: 1H-imidazole / dichloromethane / 1 h / 25 °C / Inert atmosphere

3: pyridine / 3 h / 25 °C / Inert atmosphere

With pyridine; 1H-imidazole; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0031-1289783

Reference yield:

: C₁₇H₂₄O₆

: 5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

: 1400908-42-0
5-O-acetyl-3-O-benzyl-7-O-(tert-butyldiphenylsilyl)-6-deoxy-1,2-O-isopropylidene-α-D-allo-hepto-1,4-furanose

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / dichloromethane / 1 h / 25 °C / Inert atmosphere

2: pyridine / 3 h / 25 °C / Inert atmosphere

With pyridine; 1H-imidazole; In dichloromethane;
DOI:10.1055/s-0031-1289783