acetic acid 9-[3,17β-bisbenzyloxyestra-1,3,5(10)-trien-11β-yl]-3,3,4,4,5,5,6,6-octafluorononyl ester

Base Information

• Chemical Name: acetic acid 9-[3,17β-bisbenzyloxyestra-1,3,5(10)-trien-11β-yl]-3,3,4,4,5,5,6,6-octafluorononyl ester
• CAS No.: 1104455-75-5
• Molecular Formula: C₄₃H₄₈F₈O₄
• Molecular Weight: 780.839

Synonyms:acetic acid 9-[3,17β-bisbenzyloxyestra-1,3,5(10)-trien-11β-yl]-3,3,4,4,5,5,6,6-octafluorononyl ester

Chemical Property of acetic acid 9-[3,17β-bisbenzyloxyestra-1,3,5(10)-trien-11β-yl]-3,3,4,4,5,5,6,6-octafluorononyl ester

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Technology Process of acetic acid 9-[3,17β-bisbenzyloxyestra-1,3,5(10)-trien-11β-yl]-3,3,4,4,5,5,6,6-octafluorononyl ester

There total 1 articles about acetic acid 9-[3,17β-bisbenzyloxyestra-1,3,5(10)-trien-11β-yl]-3,3,4,4,5,5,6,6-octafluorononyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

acetic acid 3,3,4,4,5,5,6,6-octafluoro-1,6-diiodohexyl ester (1104455-66-4) + 11β-allyl-3,17β-dibenzyloxyestra-1,3,5(10)-triene (534572-62-8) → acetic acid 9-[3,17β-bisbenzyloxyestra-1,3,5(10)-trien-11β-yl]-3,3,4,4,5,5,6,6-octafluorononyl ester (1104455-75-5) + acetic acid 7-[1,11β-ethano-3,17β-bisbenzyloxyestra-1,3,5(10)-trien-1'-yl]-3,3,4,4,5,5,6,6-octafluoroheptyl ester

Guidance literature:

acetic acid 3,3,4,4,5,5,6,6-octafluoro-1,6-diiodohexyl ester; 11β-allyl-3,17β-dibenzyloxyestra-1,3,5(10)-triene; With triethyl borane; In hexane; 1,2-dichloro-ethane; at 20 ℃; for 1.58333h;

With triethyl borane; triphenylstannane; In 1,2-dichloro-ethane; at 20 ℃;

DOI:10.1021/jm801154q

Reference yield: 98.0%

acetic acid 9-[3,17β-bisbenzyloxyestra-1,3,5(10)-trien-11β-yl]-3,3,4,4,5,5,6,6-octafluorononyl ester (1104455-75-5) → 9-(3,17β-bisbenzyloxyestra-1,3,5(10)-trien-11β-yl)-3,3,4,4,5,5,6,6-octafluorononan-1-ol (1104455-88-0)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.1021/jm801154q

upstream raw materials:

acetic acid 3,3,4,4,5,5,6,6-octafluoro-1,6-diiodohexyl ester

11β-allyl-3,17β-dibenzyloxyestra-1,3,5(10)-triene

Downstream raw materials:

9-(3,17β-bisbenzyloxyestra-1,3,5(10)-trien-11β-yl)-3,3,4,4,5,5,6,6-octafluorononan-1-ol

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