Technology Process of 2,3-bis-(4'-methoxybenzyl)-sn-glycerol
There total 5 articles about 2,3-bis-(4'-methoxybenzyl)-sn-glycerol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
methanol;
Yield given;
Ambient temperature;
DOI:10.1021/ja982837o
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine; dmap / dichloromethane / Ambient temperature
2: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 2 h / Ambient temperature
3: toluene-4-sulfonic acid / methanol / Ambient temperature
With
pyridine; dmap; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja982837o
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / methanol / 2 h / Ambient temperature
2: pyridine; dmap / dichloromethane / Ambient temperature
3: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 2 h / Ambient temperature
4: toluene-4-sulfonic acid / methanol / Ambient temperature
With
pyridine; dmap; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja982837o
