4,11-dibenzyl-6-(4-nitro-benzyl)-1,4,8,11-tetraaza-bicyclo[6.6.2]hexadecane

Base Information

Chemical Name:4,11-dibenzyl-6-(4-nitro-benzyl)-1,4,8,11-tetraaza-bicyclo[6.6.2]hexadecane
CAS No.:796046-14-5
Molecular Formula:C₃₃H₄₃N₅O₂
Molecular Weight:541.737
Hs Code.:

Synonyms:4,11-dibenzyl-6-(4-nitro-benzyl)-1,4,8,11-tetraaza-bicyclo[6.6.2]hexadecane

Suppliers and Price of 4,11-dibenzyl-6-(4-nitro-benzyl)-1,4,8,11-tetraaza-bicyclo[6.6.2]hexadecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,11-dibenzyl-6-(4-nitro-benzyl)-1,4,8,11-tetraaza-bicyclo[6.6.2]hexadecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,11-dibenzyl-6-(4-nitro-benzyl)-1,4,8,11-tetraaza-bicyclo[6.6.2]hexadecane

There total 3 articles about 4,11-dibenzyl-6-(4-nitro-benzyl)-1,4,8,11-tetraaza-bicyclo[6.6.2]hexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: C₃₃H₄₁N₅O₂⁽²⁺⁾*2Br^(1-)

: 796046-14-5
4,11-dibenzyl-6-(4-nitro-benzyl)-1,4,8,11-tetraaza-bicyclo[6.6.2]hexadecane

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 336h;
DOI:10.1039/b406906d

Reference yield:

: 100-39-0
benzyl bromide

: 796046-14-5
4,11-dibenzyl-6-(4-nitro-benzyl)-1,4,8,11-tetraaza-bicyclo[6.6.2]hexadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / acetonitrile / 192 h / 20 °C

2: 78 percent / NaBH₄ / ethanol / 336 h / 20 °C

With sodium tetrahydroborate; In ethanol; acetonitrile;
DOI:10.1039/b406906d

Reference yield:

: 694527-20-3
cis-2-(4-nitrobenzyl)decahydro-3a,5a,8a,10a-tetraazapyrene

: 796046-14-5
4,11-dibenzyl-6-(4-nitro-benzyl)-1,4,8,11-tetraaza-bicyclo[6.6.2]hexadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / acetonitrile / 192 h / 20 °C

2: 78 percent / NaBH₄ / ethanol / 336 h / 20 °C

With sodium tetrahydroborate; In ethanol; acetonitrile;
DOI:10.1039/b406906d