2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenyl-porphyrinogen

Base Information

• Chemical Name: 2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenyl-porphyrinogen
• CAS No.: 27226-53-5
• Molecular Formula: C₅₂H₅₂N₄
• Molecular Weight: 733.012

Synonyms:2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenyl-porphyrinogen

Chemical Property of 2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenyl-porphyrinogen

Chemical Property:

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Technology Process of 2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenyl-porphyrinogen

There total 2 articles about 2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenyl-porphyrinogen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dimethyl-1H-pyrrole (822-51-5) + benzaldehyde (100-52-7) → 2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenyl-porphyrinogen (27226-53-5)

Guidance literature:

With boron trifluoride diethyl etherate; Multistep reaction; 1.) CH₂Cl₂, RT, 15 min, 2.) 1 h;

DOI:10.1021/ja00180a029

Reference yield:

→ 2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenyl-porphyrinogen (27226-53-5)

Guidance literature:

3,4-Dimethylpyrrol,Benzaldehyd unter Luftabschluss;

Reference yield:

2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenyl-porphyrinogen (27226-53-5) → 2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin (22112-91-0)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 0.5h; Heating;

DOI:10.1021/ja00180a029

upstream raw materials:

3,4-dimethyl-1H-pyrrole

benzaldehyde

Downstream raw materials:

2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphyrin

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