C₂₅H₂₇F₃O₇

Base Information

Chemical Name:C₂₅H₂₇F₃O₇
CAS No.:1448848-30-3
Molecular Formula:C₂₅H₂₇F₃O₇
Molecular Weight:496.48
Hs Code.:

C<sub>25</sub>H<sub>27</sub>F<sub>3</sub>O<sub>7</sub>

Synonyms:C₂₅H₂₇F₃O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₇F₃O₇

Chemical Property:

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Technology Process of C₂₅H₂₇F₃O₇

There total 4 articles about C₂₅H₂₇F₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1448848-24-5
(R,E)-ethyl5-(3,4-dimethoxyphenyl)-4-hydroxypent-2-enoate

: 17257-71-5,20445-31-2,56135-03-6,81655-41-6
(S)-Mosher acid

: 1448848-30-3
C₂₅H₂₇F₃O₇

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 13h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.06.034

Reference yield:

: 3929-47-3
3-(3,4-dimethoxyphenyl)-1-propanol

: 1448848-30-3
C₂₅H₂₇F₃O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; dimethyl sulfoxide / dichloromethane / 3 h / 20 °C

2.1: Nitrosobenzene; L-proline / dimethyl sulfoxide / 0.42 h / 20 °C / Inert atmosphere

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 13 h / 20 °C / Inert atmosphere

With dmap; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; Nitrosobenzene; dicyclohexyl-carbodiimide; L-proline; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; dimethyl sulfoxide; acetonitrile; 2.1: |Horner-Wadsworth-Emmons Olefination / 3.1: |Horner-Wadsworth-Emmons Olefination / 3.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.tetlet.2013.06.034

Reference yield:

: 61871-67-8
3-(3,4-Dimethoxyphenyl)propanal

: 1448848-30-3
C₂₅H₂₇F₃O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: Nitrosobenzene; L-proline / dimethyl sulfoxide / 0.42 h / 20 °C / Inert atmosphere

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 13 h / 20 °C / Inert atmosphere

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; Nitrosobenzene; dicyclohexyl-carbodiimide; L-proline; lithium chloride; In dichloromethane; dimethyl sulfoxide; acetonitrile; 1.1: |Horner-Wadsworth-Emmons Olefination / 2.1: |Horner-Wadsworth-Emmons Olefination / 2.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.tetlet.2013.06.034