(Z)-4,4,5,5-tetramethyl-2-(1,2,3-triphenylpenta-1,4-dien-1-yl)-1,3,2-dioxaborolane

Base Information

Chemical Name:(Z)-4,4,5,5-tetramethyl-2-(1,2,3-triphenylpenta-1,4-dien-1-yl)-1,3,2-dioxaborolane
CAS No.:1419186-06-3
Molecular Formula:C₂₉H₃₁BO₂
Molecular Weight:422.375
Hs Code.:

Synonyms:(Z)-4,4,5,5-tetramethyl-2-(1,2,3-triphenylpenta-1,4-dien-1-yl)-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-4,4,5,5-tetramethyl-2-(1,2,3-triphenylpenta-1,4-dien-1-yl)-1,3,2-dioxaborolane

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Technology Process of (Z)-4,4,5,5-tetramethyl-2-(1,2,3-triphenylpenta-1,4-dien-1-yl)-1,3,2-dioxaborolane

There total 2 articles about (Z)-4,4,5,5-tetramethyl-2-(1,2,3-triphenylpenta-1,4-dien-1-yl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1240492-12-9
(Z)-C₆H₅CHCHCH₂OP(O-iPr)2O

: 501-65-5
diphenyl acetylene

: 73183-34-3
bis(pinacol)diborane

: 1419186-06-3
(Z)-4,4,5,5-tetramethyl-2-(1,2,3-triphenylpenta-1,4-dien-1-yl)-1,3,2-dioxaborolane

Guidance literature:: With potassium tert-butylate; copper(l) chloride; tricyclohexylphosphine; In toluene; at 50 ℃; for 20h; regioselective reaction;
DOI:10.1021/acscatal.5b01441

Reference yield: 51.0%

: bis(pinacolato)diborane

: 501-65-5
diphenyl acetylene

: diethyl 3-phenylprop-2-enyl phosphate

: 1419186-06-3
(Z)-4,4,5,5-tetramethyl-2-(1,2,3-triphenylpenta-1,4-dien-1-yl)-1,3,2-dioxaborolane

Guidance literature:: With potassium tert-butylate; copper diacetate; tricyclohexylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; at 50 ℃; for 40h; stereoselective reaction; Schlenk technique;
DOI:10.1021/ol4001526