1-phthalimido-n'-(2,6-dichlorobenzoyl)ferrocene

Base Information

Chemical Name:1-phthalimido-n'-(2,6-dichlorobenzoyl)ferrocene
CAS No.:920758-28-7
Molecular Formula:C₂₅H₁₅Cl₂FeNO₃
Molecular Weight:504.152
Hs Code.:

Synonyms:1-phthalimido-n'-(2,6-dichlorobenzoyl)ferrocene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phthalimido-n'-(2,6-dichlorobenzoyl)ferrocene

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Technology Process of 1-phthalimido-n'-(2,6-dichlorobenzoyl)ferrocene

There total 1 articles about 1-phthalimido-n'-(2,6-dichlorobenzoyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1294-21-9
N-ferrocenyl phthalimide

: 4659-45-4
2,6-Dichlorobenzoyl chloride

: 920758-28-7
1-phthalimido-n'-(2,6-dichlorobenzoyl)ferrocene

Guidance literature:: With AlCl₃; In dichloromethane; (Ar or N2); using Schlenk techiques; treatment of soln. of 2-ferrocenylisoindole-1,3-dione in CH2Cl2 with 2,6-dichlorobenzoyl chloride and AlCl3at 0°C; stirring at 0°C for 30 min and at room temp. for 14 h; cooling to 0°C; extn. with CH2Cl2; washing with H2O and 10% aq. NaOH; drying over MgSO4; filtration, evapn. to dryness; recrystn. from Et2O; elem. anal.;

Reference yield: 86.0%

: 920758-28-7
1-phthalimido-n'-(2,6-dichlorobenzoyl)ferrocene

: 920758-29-8
1-amino-n'-(2,6-dichlorobenzoyl)ferrocene

Guidance literature:: With hydrazine monohydrate; In ethanol; (Ar or N2); using Schlenk techniques; dissolving of 1-phthalimido-1'-(2,6-dichlorobenzoyl)-ferrocene in EtOH; addn. of hydrazine monohydrate; reflux for 2 h; cooling to ambient temp., addn. of H2O; extn. with Et2O; drying of combined org. phases over Na2SO4; filtration, evapn. to dryness under reducedpressure; elem. anal.;