[[5-bromo-2-(trifluoroacetamido)phenyl]methyl]triphenylphosphanium bromide

Base Information

Chemical Name:[[5-bromo-2-(trifluoroacetamido)phenyl]methyl]triphenylphosphanium bromide
CAS No.:837392-59-3
Molecular Formula:Br*C₂₇H₂₁BrF₃NOP
Molecular Weight:623.247
Hs Code.:

Synonyms:[[5-bromo-2-(trifluoroacetamido)phenyl]methyl]triphenylphosphanium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [[5-bromo-2-(trifluoroacetamido)phenyl]methyl]triphenylphosphanium bromide

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Technology Process of [[5-bromo-2-(trifluoroacetamido)phenyl]methyl]triphenylphosphanium bromide

There total 4 articles about [[5-bromo-2-(trifluoroacetamido)phenyl]methyl]triphenylphosphanium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 837392-59-3
[[5-bromo-2-(trifluoroacetamido)phenyl]methyl]triphenylphosphanium bromide

Guidance literature:

Reference yield: 52.0%

: 603-35-0
triphenylphosphine

: 183173-44-6
N-[4-bromo-2-(bromomethyl)phenyl]-2,2,2-trifluoroacetamide

: 837392-59-3
[[5-bromo-2-(trifluoroacetamido)phenyl]methyl]triphenylphosphanium bromide

Guidance literature:: In toluene; at 70 ℃; for 3h;

Reference yield:

: 583-75-5
4-Bromo-2-methylaniline

: 837392-59-3
[[5-bromo-2-(trifluoroacetamido)phenyl]methyl]triphenylphosphanium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 1 h / 30 °C

2: N-Bromosuccinimide / tetrachloromethane / 6 h / Reflux; Irradiation

3: toluene / 3 h / 70 °C

With N-Bromosuccinimide; In tetrachloromethane; dichloromethane; toluene;