2-(4-(10-bromodecyloxy)phenyl)-1,4-dihydro-1,4-dioxonaphthalen-3-yl acetate

Base Information

Chemical Name:2-(4-(10-bromodecyloxy)phenyl)-1,4-dihydro-1,4-dioxonaphthalen-3-yl acetate
CAS No.:1402666-07-2
Molecular Formula:C₂₈H₃₁BrO₅
Molecular Weight:527.455
Hs Code.:

Synonyms:2-(4-(10-bromodecyloxy)phenyl)-1,4-dihydro-1,4-dioxonaphthalen-3-yl acetate

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Chemical Property of 2-(4-(10-bromodecyloxy)phenyl)-1,4-dihydro-1,4-dioxonaphthalen-3-yl acetate

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Technology Process of 2-(4-(10-bromodecyloxy)phenyl)-1,4-dihydro-1,4-dioxonaphthalen-3-yl acetate

There total 5 articles about 2-(4-(10-bromodecyloxy)phenyl)-1,4-dihydro-1,4-dioxonaphthalen-3-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1402666-05-0
2-(4-(10-bromodecyloxy)phenyl)-3-hydroxynaphthalene-1,4-dione

: 75-36-5
acetyl chloride

: 1402666-07-2
2-(4-(10-bromodecyloxy)phenyl)-1,4-dihydro-1,4-dioxonaphthalen-3-yl acetate

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1021/ml300242v

Reference yield:

: 143773-73-3
4-(10-bromo-n-decyloxy)benzaldehyde

: 1402666-07-2
2-(4-(10-bromodecyloxy)phenyl)-1,4-dihydro-1,4-dioxonaphthalen-3-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / chloroform / Reflux

2: 2,6-dimethylpyridine / dichloromethane / 1.5 h / 20 °C

With 2,6-dimethylpyridine; boron trifluoride diethyl etherate; In dichloromethane; chloroform;
DOI:10.1021/ml300242v

Reference yield:

: 83-72-7
2-hydroxynaphtho-1,4-quinone

: 1402666-07-2
2-(4-(10-bromodecyloxy)phenyl)-1,4-dihydro-1,4-dioxonaphthalen-3-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: chloroform / 9 h / 0 - 20 °C

2: boron trifluoride diethyl etherate / chloroform / Reflux

3: 2,6-dimethylpyridine / dichloromethane / 1.5 h / 20 °C

With 2,6-dimethylpyridine; boron trifluoride diethyl etherate; In dichloromethane; chloroform;
DOI:10.1021/ml300242v