methyl (methyl 5-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate 4-(diphenyl phosphate)

Base Information

Chemical Name:methyl (methyl 5-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate 4-(diphenyl phosphate)
CAS No.:116390-95-5
Molecular Formula:C₃₂H₃₇O₁₁P
Molecular Weight:628.613
Hs Code.:

Synonyms:methyl (methyl 5-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate 4-(diphenyl phosphate)

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Chemical Property of methyl (methyl 5-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate 4-(diphenyl phosphate)

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Technology Process of methyl (methyl 5-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate 4-(diphenyl phosphate)

There total 2 articles about methyl (methyl 5-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate 4-(diphenyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 116464-73-4
methyl (methyl 5-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 116390-95-5
methyl (methyl 5-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate 4-(diphenyl phosphate)

Guidance literature:: With pyridine; dmap; In benzene; for 1h;

Reference yield:

: 76249-75-7
methyl (methyl 5-O-benzyl-3-deoxy-α-D-manno-oct-2-ulopyranosid)onate

: 116390-95-5
methyl (methyl 5-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate 4-(diphenyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / toluene-p-sulphonic acid (PTSA) / acetonitrile; dimethylformamide / 0.5 h / 40 °C

2: 67 percent / pyridine, 4-dimethyl-aminopyridine (DMAP) / benzene / 1 h

With pyridine; dmap; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; acetonitrile; benzene;