2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate

Base Information

Chemical Name:2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate
CAS No.:1363399-39-6
Molecular Formula:C₁₆H₁₆ClN₃O₃S
Molecular Weight:365.84
Hs Code.:

Synonyms:2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate

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Chemical Property of 2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate

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Technology Process of 2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate

There total 2 articles about 2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 491593-46-5
N-[(6-chloropyridin-3-yl)methyl]cyanamide

: 6315-52-2
1,2-bis-tosyloxyethane

: 1363399-39-6
2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate

Guidance literature:: With sodium hydride; potassium iodide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1.33333h; Cooling with ice;

Reference yield:

: 97004-04-1
5-(aminomethyl)-2-chloropyridine

: 1363399-39-6
2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: bromocyane / chloroform / 1 h / 0 °C

2: sodium hydride; potassium iodide / N,N-dimethyl-formamide; mineral oil / 1.33 h / 20 °C / Cooling with ice

With bromocyane; sodium hydride; potassium iodide; In chloroform; N,N-dimethyl-formamide; mineral oil;

Reference yield: 72.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1363399-39-6
2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate

: 14321-27-8
N-ethylbenzylamine

: 1363399-40-9
2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl benzyl(ethyl)carbamodithioate

Guidance literature:: N-ethylbenzylamine; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.333333h;

carbon disulfide; 2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate; With potassium iodide; In tetrahydrofuran; at 40 ℃; for 1h;