2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl benzyl(ethyl)carbamodithioate

Base Information

Chemical Name:2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl benzyl(ethyl)carbamodithioate
CAS No.:1363399-40-9
Molecular Formula:C₁₉H₂₁ClN₄S₂
Molecular Weight:404.988
Hs Code.:

Synonyms:2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl benzyl(ethyl)carbamodithioate

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Chemical Property of 2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl benzyl(ethyl)carbamodithioate

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Technology Process of 2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl benzyl(ethyl)carbamodithioate

There total 3 articles about 2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl benzyl(ethyl)carbamodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1363399-39-6
2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate

: 14321-27-8
N-ethylbenzylamine

: 1363399-40-9
2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl benzyl(ethyl)carbamodithioate

Guidance literature:: N-ethylbenzylamine; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.333333h;

carbon disulfide; 2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl 4-methylbenzenesulfonate; With potassium iodide; In tetrahydrofuran; at 40 ℃; for 1h;

Reference yield:

: 97004-04-1
5-(aminomethyl)-2-chloropyridine

: 1363399-40-9
2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl benzyl(ethyl)carbamodithioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromocyane / chloroform / 1 h / 0 °C

2.1: sodium hydride; potassium iodide / N,N-dimethyl-formamide; mineral oil / 1.33 h / 20 °C / Cooling with ice

3.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / 20 °C

3.2: 1 h / 40 °C

With bromocyane; potassium tert-butylate; sodium hydride; potassium iodide; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 491593-46-5
N-[(6-chloropyridin-3-yl)methyl]cyanamide

: 1363399-40-9
2-[N-(6-chloro-3-pyridylmethyl)cyanamide]ethyl benzyl(ethyl)carbamodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride; potassium iodide / N,N-dimethyl-formamide; mineral oil / 1.33 h / 20 °C / Cooling with ice

2.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / 20 °C

2.2: 1 h / 40 °C

With potassium tert-butylate; sodium hydride; potassium iodide; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;