1-(2-(2-(2,6-dichlorophenylamino)phenyl)acetyl)-4-p-tolylthiosemicarbazide

Base Information

• Chemical Name: 1-(2-(2-(2,6-dichlorophenylamino)phenyl)acetyl)-4-p-tolylthiosemicarbazide
• CAS No.: 740799-50-2
• Molecular Formula: C₂₂H₂₀Cl₂N₄OS
• Molecular Weight: 459.399

Synonyms:1-(2-(2-(2,6-dichlorophenylamino)phenyl)acetyl)-4-p-tolylthiosemicarbazide

Chemical Property of 1-(2-(2-(2,6-dichlorophenylamino)phenyl)acetyl)-4-p-tolylthiosemicarbazide

Chemical Property:

Purity/Quality:

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Technology Process of 1-(2-(2-(2,6-dichlorophenylamino)phenyl)acetyl)-4-p-tolylthiosemicarbazide

There total 2 articles about 1-(2-(2-(2,6-dichlorophenylamino)phenyl)acetyl)-4-p-tolylthiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1-isothiocyanato-4-methylbenzene (622-59-3) + N-amino-2-{2'-[(2'',6''-dichlorophenyl)amino]phenyl}acetamide (133239-50-6) → 1-(2-(2-(2,6-dichlorophenylamino)phenyl)acetyl)-4-p-tolylthiosemicarbazide (740799-50-2)

Guidance literature:

In ethanol; for 8h; Heating;

DOI:10.1016/j.ejmech.2004.02.008

Reference yield:

ethyl 2-[2-(2,6-dichlorophenylamino)phenyl]acetate (15307-77-4) → 1-(2-(2-(2,6-dichlorophenylamino)phenyl)acetyl)-4-p-tolylthiosemicarbazide (740799-50-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / hydrazine hydrate / ethanol / 20 h / Heating

2: 68 percent / ethanol / 8 h / Heating

With hydrazine hydrate; In ethanol;

DOI:10.1016/j.ejmech.2004.02.008

Reference yield: 79.0%

1-(2-(2-(2,6-dichlorophenylamino)phenyl)acetyl)-4-p-tolylthiosemicarbazide (740799-50-2) → 5-[2-(2,6-dichlorophenylamino)benzyl]-4-p-tolyl-4H-1,2,4-triazole-3-thiol

Guidance literature:

With sodium hydroxide; In ethanol; water; for 2h; Heating;

DOI:10.1016/j.ejmech.2004.02.008

upstream raw materials:

1-isothiocyanato-4-methylbenzene

N-amino-2-{2'-[(2'',6''-dichlorophenyl)amino]phenyl}acetamide

ethyl 2-[2-(2,6-dichlorophenylamino)phenyl]acetate

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