1-(2-(3-(4-(2-(isopropyloxy)ethoxy)phenoxy)-2-hydroxypropylamino)ethyl)-3-(4-hydroxyphenyl)urea

Base Information

Chemical Name:1-(2-(3-(4-(2-(isopropyloxy)ethoxy)phenoxy)-2-hydroxypropylamino)ethyl)-3-(4-hydroxyphenyl)urea
CAS No.:1354966-87-2
Molecular Formula:C₂₃H₃₃N₃O₆
Molecular Weight:447.532
Hs Code.:

Synonyms:1-(2-(3-(4-(2-(isopropyloxy)ethoxy)phenoxy)-2-hydroxypropylamino)ethyl)-3-(4-hydroxyphenyl)urea

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Chemical Property of 1-(2-(3-(4-(2-(isopropyloxy)ethoxy)phenoxy)-2-hydroxypropylamino)ethyl)-3-(4-hydroxyphenyl)urea

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Technology Process of 1-(2-(3-(4-(2-(isopropyloxy)ethoxy)phenoxy)-2-hydroxypropylamino)ethyl)-3-(4-hydroxyphenyl)urea

There total 7 articles about 1-(2-(3-(4-(2-(isopropyloxy)ethoxy)phenoxy)-2-hydroxypropylamino)ethyl)-3-(4-hydroxyphenyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 30311-33-2
2-((4-(2-isopropoxyethoxy)phenoxy)methyl)oxirane

: 1229609-95-3
1-(2-aminoethyl)-3-(4-hydroxy)phenylurea

: 1354966-87-2
1-(2-(3-(4-(2-(isopropyloxy)ethoxy)phenoxy)-2-hydroxypropylamino)ethyl)-3-(4-hydroxyphenyl)urea

Guidance literature:: In water; isopropyl alcohol; acetonitrile; at 90 ℃; under 12929 Torr; MW reactor;

Reference yield:

: 109-59-1
2-(1-methylethoxy)-ethanol

: 1354966-87-2
1-(2-(3-(4-(2-(isopropyloxy)ethoxy)phenoxy)-2-hydroxypropylamino)ethyl)-3-(4-hydroxyphenyl)urea

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / dichloromethane / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 16 h / 20 °C

3.1: sodium hydroxide / water / 0.5 h / 40 °C / pH 14

3.2: 24.75 h / 20 - 60 °C

4.1: isopropyl alcohol; acetonitrile; water / 90 °C / 12929 Torr / MW reactor

With di-isopropyl azodicarboxylate; hydrogen; triphenylphosphine; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol; acetonitrile;

Reference yield:

: 103-16-2
4-Benzyloxyphenol

: 1354966-87-2
1-(2-(3-(4-(2-(isopropyloxy)ethoxy)phenoxy)-2-hydroxypropylamino)ethyl)-3-(4-hydroxyphenyl)urea

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / dichloromethane / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 16 h / 20 °C

3.1: sodium hydroxide / water / 0.5 h / 40 °C / pH 14

3.2: 24.75 h / 20 - 60 °C

4.1: isopropyl alcohol; acetonitrile; water / 90 °C / 12929 Torr / MW reactor

With di-isopropyl azodicarboxylate; hydrogen; triphenylphosphine; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol; acetonitrile;