(3S)-3-(1-(benzo[d]thiazol-2-ylsulfonyl)-2-oxo-2-p-tolylethyl)cyclohexanone

Base Information

Chemical Name:(3S)-3-(1-(benzo[d]thiazol-2-ylsulfonyl)-2-oxo-2-p-tolylethyl)cyclohexanone
CAS No.:1196132-37-2
Molecular Formula:C₂₂H₂₁NO₄S₂
Molecular Weight:427.545
Hs Code.:

Synonyms:(3S)-3-(1-(benzo[d]thiazol-2-ylsulfonyl)-2-oxo-2-p-tolylethyl)cyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S)-3-(1-(benzo[d]thiazol-2-ylsulfonyl)-2-oxo-2-p-tolylethyl)cyclohexanone

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Technology Process of (3S)-3-(1-(benzo[d]thiazol-2-ylsulfonyl)-2-oxo-2-p-tolylethyl)cyclohexanone

There total 1 articles about (3S)-3-(1-(benzo[d]thiazol-2-ylsulfonyl)-2-oxo-2-p-tolylethyl)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 930-68-7
cyclohexenone

: 1196132-27-0
2-(benzo[d]thiazol-2-ylsulfonyl)-1-p-tolylethanone

: 1196132-37-2
(3S)-3-(1-(benzo[d]thiazol-2-ylsulfonyl)-2-oxo-2-p-tolylethyl)cyclohexanone

Guidance literature:: With 9-amino(9-deoxy)epiquinidine di(trifluoroacetic acid); In 1,4-dioxane; at 20 ℃; for 24h; enantioselective reaction;
DOI:10.1002/anie.200903790

Reference yield:

: 1196132-37-2
(3S)-3-(1-(benzo[d]thiazol-2-ylsulfonyl)-2-oxo-2-p-tolylethyl)cyclohexanone

: Z-(1S,3S)-3-(2-p-tolyl-vinyl)-cyclohexanol

: 1196132-49-6
E-(1S,3S)-3-(2-p-tolyl-vinyl)-cyclohexanol

Guidance literature:: (3S)-3-(1-(benzo[d]thiazol-2-ylsulfonyl)-2-oxo-2-p-tolylethyl)cyclohexanone; With sodium tetrahydroborate; In methanol; toluene; at -30 ℃;

With ammonium chloride; In methanol; water; toluene; optical yield given as %de; enantioselective reaction;
DOI:10.1002/anie.200903790

Reference yield:

: 1196132-37-2
(3S)-3-(1-(benzo[d]thiazol-2-ylsulfonyl)-2-oxo-2-p-tolylethyl)cyclohexanone

: 1228358-61-9
(1S,4S)-6-p-tolylbicyclo[2.2.2]oct-5-en-2-one

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium carbonate; In water; toluene; at 45 ℃; for 24h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/chem.200903274