2-butyl-1-(2-oxo-4S-phenyl-oxazolidine-3-carbonyl)-cycloprop-2-ene carbonyl azide

Base Information

Chemical Name:2-butyl-1-(2-oxo-4S-phenyl-oxazolidine-3-carbonyl)-cycloprop-2-ene carbonyl azide
CAS No.:905845-46-7
Molecular Formula:C₁₈H₁₈N₄O₄
Molecular Weight:354.365
Hs Code.:

Synonyms:2-butyl-1-(2-oxo-4S-phenyl-oxazolidine-3-carbonyl)-cycloprop-2-ene carbonyl azide

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Chemical Property of 2-butyl-1-(2-oxo-4S-phenyl-oxazolidine-3-carbonyl)-cycloprop-2-ene carbonyl azide

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Technology Process of 2-butyl-1-(2-oxo-4S-phenyl-oxazolidine-3-carbonyl)-cycloprop-2-ene carbonyl azide

There total 4 articles about 2-butyl-1-(2-oxo-4S-phenyl-oxazolidine-3-carbonyl)-cycloprop-2-ene carbonyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 905845-32-1
pentafluorophenyl 2-butyl-1-(2-oxo-4S-phenyl-oxazolidine-3-carbonyl)-cycloprop-2-ene carboxylic ester

: 905845-46-7
2-butyl-1-(2-oxo-4S-phenyl-oxazolidine-3-carbonyl)-cycloprop-2-ene carbonyl azide

Guidance literature:: With dmap; sodium azide; In tetrahydrofuran; water; at 20 ℃; for 15h;
DOI:10.1021/ol060847l

Reference yield:

: 905845-02-5
2-butyl-cycloprop-2-ene-1,1-dicarboxylic acid

: 905845-46-7
2-butyl-1-(2-oxo-4S-phenyl-oxazolidine-3-carbonyl)-cycloprop-2-ene carbonyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / ethyldiisopropylamine / CH₂Cl₂ / 0.5 h / cooling

2: 90 percent / tetrahydrofuran; pentane; CH₂Cl₂ / -78 - 20 °C

3: 97 percent / NaN₃; DMAP / tetrahydrofuran; H₂O / 15 h / 20 °C

With dmap; sodium azide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; pentane;
DOI:10.1021/ol060847l

Reference yield:

: 905845-18-3
bis-pentafluorophenyl 2-butyl-cycloprop-2-ene-1,1-bis-carboxylic ester

: 905845-46-7
2-butyl-1-(2-oxo-4S-phenyl-oxazolidine-3-carbonyl)-cycloprop-2-ene carbonyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / tetrahydrofuran; pentane; CH₂Cl₂ / -78 - 20 °C

2: 97 percent / NaN₃; DMAP / tetrahydrofuran; H₂O / 15 h / 20 °C

With dmap; sodium azide; In tetrahydrofuran; dichloromethane; water; pentane;
DOI:10.1021/ol060847l