Technology Process of C35H32BrN3O4S
There total 8 articles about C35H32BrN3O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C29H28BrN3O2;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 0 ℃;
for 0.5h;
Inert atmosphere;
benzenesulfonyl chloride;
In
tetrahydrofuran; mineral oil;
at 0 ℃;
DOI:10.1021/ol202475r
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: toluene / Reflux
2.1: pyridinium perbromide hydrobromide / tetrahydrofuran; chloroform / 2.33 h / -10 °C
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C
3.2: 4 h / 0 - 20 °C
4.1: hydrazine hydrate / ethanol / Reflux
5.1: methanol / 24 h / 20 °C
6.1: boron trifluoride diethyl etherate / tetrahydrofuran; dichloromethane / 0.25 h / -40 °C / Inert atmosphere
6.2: 4 h / -40 - 20 °C
7.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere
7.2: 0 °C
With
pyridinium perbromide hydrobromide; boron trifluoride diethyl etherate; sodium hydride; hydrazine hydrate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ol202475r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: methanol / 24 h / 20 °C
2.1: boron trifluoride diethyl etherate / tetrahydrofuran; dichloromethane / 0.25 h / -40 °C / Inert atmosphere
2.2: 4 h / -40 - 20 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere
3.2: 0 °C
With
boron trifluoride diethyl etherate; sodium hydride;
In
tetrahydrofuran; methanol; dichloromethane; mineral oil;
DOI:10.1021/ol202475r
