3-(1-{2-[3-(tert-Butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl}-1H-indol-3-yl)-4-(1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione

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Chemical Name:3-(1-{2-[3-(tert-Butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl}-1H-indol-3-yl)-4-(1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione
CAS No.:203250-14-0
Molecular Formula:C₆₂H₅₉N₃O₅Si
Molecular Weight:954.253
Hs Code.:

Synonyms:3-(1-{2-[3-(tert-Butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl}-1H-indol-3-yl)-4-(1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione

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Chemical Property of 3-(1-{2-[3-(tert-Butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl}-1H-indol-3-yl)-4-(1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione

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Technology Process of 3-(1-{2-[3-(tert-Butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl}-1H-indol-3-yl)-4-(1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione

There total 1 articles about 3-(1-{2-[3-(tert-Butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl}-1H-indol-3-yl)-4-(1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 113963-68-1
bisindolylmaleimide V

: 203250-11-7
Methanesulfonic acid 2-[3-(tert-butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl ester

: 3,4-Bis-(1-{2-[3-(tert-butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl}-1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione

: 203250-14-0
3-(1-{2-[3-(tert-Butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl}-1H-indol-3-yl)-4-(1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 24h;
DOI:10.1021/jo971980h

Reference yield: 89.0%

: 203250-14-0
3-(1-{2-[3-(tert-Butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl}-1H-indol-3-yl)-4-(1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione

: 203250-17-3
3-{1-[2-(3-Hydroxy-1-trityloxymethyl-propoxy)-ethyl]-1H-indol-3-yl}-4-(1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 1.5h;
DOI:10.1021/jo971980h

Reference yield:

: 203250-14-0
3-(1-{2-[3-(tert-Butyl-diphenyl-silanyloxy)-1-trityloxymethyl-propoxy]-ethyl}-1H-indol-3-yl)-4-(1H-indol-3-yl)-1-methyl-pyrrole-2,5-dione

: 203250-18-4
Methanesulfonic acid 3-(2-{3-[4-(1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]-indol-1-yl}-ethoxy)-4-trityloxy-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1.5 h

2: 100 percent / triethylamine / CH₂Cl₂ / 0.5 h / 0 °C

With tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo971980h