S-phenyl thio-n-valerate

Base Information

• Chemical Name: S-phenyl thio-n-valerate
• CAS No.: 56379-68-1
• Molecular Formula: C₁₁H₁₄OS
• Molecular Weight: 194.298
• Mol file: 56379-68-1.mol

Synonyms:S-phenyl thio-n-valerate

Chemical Property of S-phenyl thio-n-valerate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of S-phenyl thio-n-valerate

There total 14 articles about S-phenyl thio-n-valerate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

n-valeryl chloride (638-29-9) + thiophenol (108-98-5) → S-phenyl thio-n-valerate (56379-68-1)

Guidance literature:

With tetrabutyl-ammonium chloride; sodium hydroxide; In dichloromethane; water; at 0 ℃; for 0.0833333h;

DOI:10.1080/10426501003713072

Reference yield: 84.0%

pentanal (110-62-3) + diphenyldisulfane (882-33-7) → S-phenyl thio-n-valerate (56379-68-1)

Guidance literature:

With dipotassium peroxodisulfate; tetraethylammonium bromide; In 1,2-dichloro-ethane; at 90 ℃; for 40h; Inert atmosphere;

DOI:10.1002/adsc.201300584

Reference yield: 82.0%

pentanal (110-62-3) + thiophenol (108-98-5) → S-phenyl thio-n-valerate (56379-68-1)

Guidance literature:

With dipotassium peroxodisulfate; tetraethylammonium bromide; In 1,2-dichloro-ethane; at 90 ℃; for 40h; Inert atmosphere;

DOI:10.1002/adsc.201300584

upstream raw materials:

1-cyclohexene

n-valeryl chloride

thiophenol

methyl phenyl sulfide α-carbanion

Downstream raw materials:

1-phenylthio-1-pentenyl diphenyl phosphate

N,N-dimethylpentanamide

n-hexan-2-one

1-methyl-1-pentenyl phenyl sulfide