bis[(5,5'-10,20-bis[2,6-bis(3,3-dimethyl-1-butyloxy)phenyl]porphyrinato)zinc(II)]ethyne

Base Information

• Chemical Name: bis[(5,5'-10,20-bis[2,6-bis(3,3-dimethyl-1-butyloxy)phenyl]porphyrinato)zinc(II)]ethyne
• CAS No.: 333363-20-5
• Molecular Formula: C₁₁₄H₁₃₄N₈O₈Zn₂
• Molecular Weight: 1875.15

Synonyms:bis[(5,5'-10,20-bis[2,6-bis(3,3-dimethyl-1-butyloxy)phenyl]porphyrinato)zinc(II)]ethyne

Chemical Property of bis[(5,5'-10,20-bis[2,6-bis(3,3-dimethyl-1-butyloxy)phenyl]porphyrinato)zinc(II)]ethyne

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Technology Process of bis[(5,5'-10,20-bis[2,6-bis(3,3-dimethyl-1-butyloxy)phenyl]porphyrinato)zinc(II)]ethyne

There total 1 articles about bis[(5,5'-10,20-bis[2,6-bis(3,3-dimethyl-1-butyloxy)phenyl]porphyrinato)zinc(II)]ethyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(5-ethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphyrinato)zinc(II) (478184-27-9) + [5-bromo-10,20-bis(2’,6’-bis(3”,3”-dimethylbutoxy)phenyl)porphinato]zinc(II) (478184-34-8) → bis[(5,5'-10,20-bis[2,6-bis(3,3-dimethyl-1-butyloxy)phenyl]porphyrinato)zinc(II)]ethyne (333363-20-5)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; triethylamine; In tetrahydrofuran; at 60 ℃; for 14h;

DOI:10.1021/jp102901u

Reference yield: 85.0%

bis[(5,5'-10,20-bis[2,6-bis(3,3-dimethyl-1-butyloxy)phenyl]porphyrinato)zinc(II)]ethyne (333363-20-5) → bis(5,5'-10,20-bis[2,6-bis(3,3-dimethyl-1-butyloxy)phenyl]porphyrin)ethyne

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 0.5h;

DOI:10.1021/jacs.7b03252

Reference yield:

bis[(5,5'-10,20-bis[2,6-bis(3,3-dimethyl-1-butyloxy)phenyl]porphyrinato)zinc(II)]ethyne (333363-20-5) → C114H138N8O8

Guidance literature:

With trifluoroacetic acid; In chloroform; for 0.5h;

DOI:10.1021/jp102901u

upstream raw materials:

(5-ethynyl-10,20-bis(2',6'-bis(3,3-dimethyl-1-butyloxy)phenyl)porphyrinato)zinc(II)

[5-bromo-10,20-bis(2’,6’-bis(3”,3”-dimethylbutoxy)phenyl)porphinato]zinc(II)

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