2-(p-methylphenylaminosulfonylmethyl)-5-[Z-(p-methylstyrylsulfonylmethyl)]-1,3,4-thiadiazole

Base Information

Chemical Name:2-(p-methylphenylaminosulfonylmethyl)-5-[Z-(p-methylstyrylsulfonylmethyl)]-1,3,4-thiadiazole
CAS No.:1370346-36-3
Molecular Formula:C₂₀H₂₁N₃O₄S₃
Molecular Weight:463.602
Hs Code.:

Synonyms:2-(p-methylphenylaminosulfonylmethyl)-5-[Z-(p-methylstyrylsulfonylmethyl)]-1,3,4-thiadiazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(p-methylphenylaminosulfonylmethyl)-5-[Z-(p-methylstyrylsulfonylmethyl)]-1,3,4-thiadiazole

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Technology Process of 2-(p-methylphenylaminosulfonylmethyl)-5-[Z-(p-methylstyrylsulfonylmethyl)]-1,3,4-thiadiazole

There total 4 articles about 2-(p-methylphenylaminosulfonylmethyl)-5-[Z-(p-methylstyrylsulfonylmethyl)]-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1370346-33-0
2-(p-methylphenylaminosulfonylmethyl)-5-[Z-(p-methylstyrylsulfonylmethyl)]-1,3,4-oxadiazole

: 1370346-36-3
2-(p-methylphenylaminosulfonylmethyl)-5-[Z-(p-methylstyrylsulfonylmethyl)]-1,3,4-thiadiazole

Guidance literature:: With thiourea; In tetrahydrofuran; at 120 - 130 ℃;
DOI:10.1248/cpb.59.1509

Reference yield:

: 1136056-24-0
C₁₀H₁₃NO₄S

: 1370346-36-3
2-(p-methylphenylaminosulfonylmethyl)-5-[Z-(p-methylstyrylsulfonylmethyl)]-1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; hydrazine hydrate / methanol / Reflux

2: trichlorophosphate / Reflux

3: thiourea / tetrahydrofuran / 120 - 130 °C

With pyridine; hydrazine hydrate; thiourea; trichlorophosphate; In tetrahydrofuran; methanol;
DOI:10.1248/cpb.59.1509

Reference yield:

: 1370346-31-8
C₉H₁₃N₃O₃S

: 1370346-36-3
2-(p-methylphenylaminosulfonylmethyl)-5-[Z-(p-methylstyrylsulfonylmethyl)]-1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / Reflux

2: thiourea / tetrahydrofuran / 120 - 130 °C

With thiourea; trichlorophosphate; In tetrahydrofuran;
DOI:10.1248/cpb.59.1509