ethyl 3-O-benzyl-6-deoxy-6-nitro-1,2-O-isopropyl-D,L-glycero-α-D-glucoheptofuronate

Base Information

Chemical Name:ethyl 3-O-benzyl-6-deoxy-6-nitro-1,2-O-isopropyl-D,L-glycero-α-D-glucoheptofuronate
CAS No.:95580-70-4
Molecular Formula:C₁₉H₂₅NO₉
Molecular Weight:411.409
Hs Code.:

Synonyms:ethyl 3-O-benzyl-6-deoxy-6-nitro-1,2-O-isopropyl-D,L-glycero-α-D-glucoheptofuronate

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Chemical Property of ethyl 3-O-benzyl-6-deoxy-6-nitro-1,2-O-isopropyl-D,L-glycero-α-D-glucoheptofuronate

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Technology Process of ethyl 3-O-benzyl-6-deoxy-6-nitro-1,2-O-isopropyl-D,L-glycero-α-D-glucoheptofuronate

There total 2 articles about ethyl 3-O-benzyl-6-deoxy-6-nitro-1,2-O-isopropyl-D,L-glycero-α-D-glucoheptofuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 626-35-7
nitroacetic acid ethyl ester

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 95580-70-4
ethyl 3-O-benzyl-6-deoxy-6-nitro-1,2-O-isopropyl-D,L-glycero-α-D-glucoheptofuronate

Guidance literature:: With tetrabutyl ammonium fluoride; tert-butyldimethylsilyl chloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 0.25h;
DOI:10.1016/S0957-4166(03)00274-X

Reference yield:

: 626-35-7
nitroacetic acid ethyl ester

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 95580-70-4
Ethyl-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-6-nitro-DL-glycero-α-D-gluco-heptofuranuronat

Guidance literature:: In N,N-dimethyl-formamide; for 0.5h; Yield given;
DOI:10.1002/jlac.198519850113

Reference yield: 56.0%

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 95580-70-4
ethyl 3-O-benzyl-6-deoxy-6-nitro-1,2-O-isopropyl-D,L-glycero-α-D-glucoheptofuronate

: ethyl 3,5-di-O-benzyl-6-deoxy-6-nitro-1,2-O-isopropyl-D,L-glycero-α-D-glucoheptofuronate

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; cyclohexane; at 20 ℃; for 16h;
DOI:10.1016/S0957-4166(03)00274-X