Ethyl-6-acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat

Base Information

Chemical Name:Ethyl-6-acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat
CAS No.:95580-73-7
Molecular Formula:C₂₁H₂₉NO₈
Molecular Weight:423.463
Hs Code.:

Synonyms:Ethyl-6-acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat

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Chemical Property of Ethyl-6-acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat

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Technology Process of Ethyl-6-acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat

There total 2 articles about Ethyl-6-acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.5%

: 108-24-7
acetic anhydride

: 95580-70-4
Ethyl-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-6-nitro-DL-glycero-α-D-gluco-heptofuranuronat

: 95580-71-5
Ethyl-6-acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronat

: 95580-73-7
Ethyl-6-acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat

: 95580-72-6
Ethyl-6-acetamido-5-O-acetyl-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronat

Guidance literature:: With hydrogen; nickel; for 8h; Ambient temperature;
DOI:10.1002/jlac.198519850113

Reference yield:

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 95580-73-7
Ethyl-6-acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide / 0.5 h

2: 18 percent / H₂ / Raney nickel / 8 h / Ambient temperature

With hydrogen; nickel; In N,N-dimethyl-formamide;
DOI:10.1002/jlac.198519850113