rac-benzyl (6,6,7,7,7-pentafluoro-2-hydroxy-2-methylheptan-3-yl)carbamate

Base Information

Chemical Name:rac-benzyl (6,6,7,7,7-pentafluoro-2-hydroxy-2-methylheptan-3-yl)carbamate
CAS No.:1609166-32-6
Molecular Formula:C₁₆H₂₀F₅NO₃
Molecular Weight:369.332
Hs Code.:

Synonyms:rac-benzyl (6,6,7,7,7-pentafluoro-2-hydroxy-2-methylheptan-3-yl)carbamate

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Chemical Property of rac-benzyl (6,6,7,7,7-pentafluoro-2-hydroxy-2-methylheptan-3-yl)carbamate

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Technology Process of rac-benzyl (6,6,7,7,7-pentafluoro-2-hydroxy-2-methylheptan-3-yl)carbamate

There total 4 articles about rac-benzyl (6,6,7,7,7-pentafluoro-2-hydroxy-2-methylheptan-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1609166-19-9
rac-methyl N-[(benzyloxy)carbonyl]-5,5,6,6,6-pentafluoronorleucinate

: 75-16-1
methylmagnesium bromide

: 1609166-32-6
rac-benzyl (6,6,7,7,7-pentafluoro-2-hydroxy-2-methylheptan-3-yl)carbamate

Guidance literature:: In tetrahydrofuran; diethyl ether; at 0 - 20 ℃;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1609166-32-6
rac-benzyl (6,6,7,7,7-pentafluoro-2-hydroxy-2-methylheptan-3-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water; tetrahydrofuran / 20 °C / Inert atmosphere

2: tetrahydrofuran; diethyl ether / 0 - 20 °C / Inert atmosphere

With potassium carbonate; In tetrahydrofuran; diethyl ether; water;

Reference yield:

: 1609166-18-8
methyl 2-amino-5,5,6,6,6-pentafluorohexanoate hydrochloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 1609166-32-6
rac-benzyl (6,6,7,7,7-pentafluoro-2-hydroxy-2-methylheptan-3-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran; water; dichloromethane / 20 °C / Inert atmosphere

2: tetrahydrofuran; diethyl ether / 0 - 20 °C / Inert atmosphere

With potassium carbonate; In tetrahydrofuran; diethyl ether; dichloromethane; water;