C₃₄H₄₆FN₃O₇

Base Information

Chemical Name:C₃₄H₄₆FN₃O₇
CAS No.:1009093-66-6
Molecular Formula:C₃₄H₄₆FN₃O₇
Molecular Weight:627.754
Hs Code.:

C<sub>34</sub>H<sub>46</sub>FN<sub>3</sub>O<sub>7</sub>

Synonyms:C₃₄H₄₆FN₃O₇

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Chemical Property of C₃₄H₄₆FN₃O₇

Chemical Property:

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Technology Process of C₃₄H₄₆FN₃O₇

There total 9 articles about C₃₄H₄₆FN₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1009092-10-7
C₁₅H₂₂BNO₄

: 1009093-65-5
C₂₅H₃₆BrFN₂O₅

: 1009093-66-6
C₃₄H₄₆FN₃O₇

Guidance literature:: C₁₅H₂₂BNO₄; C₂₅H₃₆BrFN₂O₅; With potassium acetate; caesium carbonate; In dimethyl sulfoxide; for 0.166667h;

(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dimethyl sulfoxide; at 70 ℃; for 4h;

Reference yield:

: 1009093-60-0
3-bromo-5-fluoro-2-methoxybenzaldehyde

: 1009093-66-6
C₃₄H₄₆FN₃O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 1 h / 20 °C

2.1: hydrogenchloride; sodium cyanoborohydride; methyl red / tetrahydrofuran; methanol; water / 12 h / pH 3

2.2: pH 9

3.1: calcium chloride / diethyl ether / 3 h / 20 °C

4.1: titanium(IV) isopropylate / tetrahydrofuran / 0.25 h / 140 °C / Microwave irradiation

4.2: 20 °C

5.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

6.1: trimethylaluminum / hexane; dichloromethane / 1 h / 20 °C

6.2: 12 h / 20 °C

6.3: 2 h

7.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.17 h

7.2: 4 h / 70 °C

With titanium(IV) isopropylate; hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate; methyl red; calcium chloride; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: C₈H₇BrFNO₂

: 1009093-66-6
C₃₄H₄₆FN₃O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; sodium cyanoborohydride; methyl red / tetrahydrofuran; methanol; water / 12 h / pH 3

1.2: pH 9

2.1: calcium chloride / diethyl ether / 3 h / 20 °C

3.1: titanium(IV) isopropylate / tetrahydrofuran / 0.25 h / 140 °C / Microwave irradiation

3.2: 20 °C

4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

5.1: trimethylaluminum / hexane; dichloromethane / 1 h / 20 °C

5.2: 12 h / 20 °C

5.3: 2 h

6.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.17 h

6.2: 4 h / 70 °C

With titanium(IV) isopropylate; hydrogenchloride; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate; methyl red; calcium chloride; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide;