3(3'R),4(R)-3-[3'-(4''-methoxyphenyl)-4'-methyl-1'-oxo-2'-pentanyl]-4-phenyl-2-oxazolidinone

Base Information

Chemical Name:3(3'R),4(R)-3-[3'-(4''-methoxyphenyl)-4'-methyl-1'-oxo-2'-pentanyl]-4-phenyl-2-oxazolidinone
CAS No.:198014-48-1
Molecular Formula:C₂₂H₂₅NO₄
Molecular Weight:367.445
Hs Code.:

Synonyms:3(3'R),4(R)-3-[3'-(4''-methoxyphenyl)-4'-methyl-1'-oxo-2'-pentanyl]-4-phenyl-2-oxazolidinone

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Chemical Property of 3(3'R),4(R)-3-[3'-(4''-methoxyphenyl)-4'-methyl-1'-oxo-2'-pentanyl]-4-phenyl-2-oxazolidinone

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Technology Process of 3(3'R),4(R)-3-[3'-(4''-methoxyphenyl)-4'-methyl-1'-oxo-2'-pentanyl]-4-phenyl-2-oxazolidinone

There total 3 articles about 3(3'R),4(R)-3-[3'-(4''-methoxyphenyl)-4'-methyl-1'-oxo-2'-pentanyl]-4-phenyl-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.4%

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 194031-58-8
(4R,2E)-3-(1-oxo-2-isohexenyl)-4-phenyl-2-oxazolidinone

: 198014-48-1
3(3'R),4(R)-3-[3'-(4''-methoxyphenyl)-4'-methyl-1'-oxo-2'-pentanyl]-4-phenyl-2-oxazolidinone

Guidance literature:: With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -78 - 20 ℃; for 3.25h;
DOI:10.1016/S0957-4166(97)00381-9

Reference yield:

: 1775-44-6,10321-71-8,16666-43-6
(2E)-4-methylpent-2-enoic acid

: 198014-48-1
3(3'R),4(R)-3-[3'-(4''-methoxyphenyl)-4'-methyl-1'-oxo-2'-pentanyl]-4-phenyl-2-oxazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / tetrahydrofuran / 1.25 h / -78 - 0 °C

2: tetrahydrofuran / 3 h / -78 - 20 °C

3: 81.4 percent / CuBr*Me₂S / tetrahydrofuran / 3.25 h / -78 - 20 °C

With copper(I) bromide dimethylsulfide complex; triethylamine; In tetrahydrofuran;
DOI:10.1016/S0957-4166(97)00381-9

Reference yield:

: C₃H₇CHCHCO₂COC₄H₉

: 198014-48-1
3(3'R),4(R)-3-[3'-(4''-methoxyphenyl)-4'-methyl-1'-oxo-2'-pentanyl]-4-phenyl-2-oxazolidinone

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 3 h / -78 - 20 °C

2: 81.4 percent / CuBr*Me₂S / tetrahydrofuran / 3.25 h / -78 - 20 °C

With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran;
DOI:10.1016/S0957-4166(97)00381-9