C₃₇H₅₀O₈Si₂

Base Information

Chemical Name:C₃₇H₅₀O₈Si₂
CAS No.:1450741-64-6
Molecular Formula:C₃₇H₅₀O₈Si₂
Molecular Weight:678.97
Hs Code.:

C<sub>37</sub>H<sub>50</sub>O<sub>8</sub>Si<sub>2</sub>

Synonyms:C₃₇H₅₀O₈Si₂

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Chemical Property of C₃₇H₅₀O₈Si₂

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Technology Process of C₃₇H₅₀O₈Si₂

There total 12 articles about C₃₇H₅₀O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1450741-62-4
(S)-5,7-bis((benzyloxy)methoxy)-3-((S)-1-hydroxyethyl)-6-((S)-2-methyl-3-oxobutyl)isobenzofuran-1(3H)-one

: 1450741-64-6
C₃₇H₅₀O₈Si₂

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol402191t

Reference yield:

: 3,5-bis((benzyloxy)methoxy)-4-bromo-1-prop-1-en-1-ylbenzene

: 1450741-64-6
C₃₇H₅₀O₈Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II) / toluene / 16 h / Inert atmosphere; Schlenk technique; Reflux

2: palladium diacetate; ruphos; potassium carbonate / toluene; water / 1.5 h / 85 °C / Inert atmosphere; Schlenk technique

3: tetrahydrofuran; diethyl ether / 0.25 h / -78 - 0 °C / Inert atmosphere; Schlenk technique

4: hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III); potassium osmate; potassium carbonate; methanesulfonamide / water; tert-butyl alcohol / 18 h / 20 °C / Inert atmosphere; Schlenk technique

5: iodine; silver trifluoroacetate / chloroform / 1.5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

6: N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 24 h / 100 °C / 760.05 Torr / Schlenk technique

7: triethylamine; dmap / dichloromethane / 0.25 h / 0 °C / Inert atmosphere; Schlenk technique

With dmap; potassium osmate; (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); tetrakis(triphenylphosphine) palladium⁽⁰⁾; methanesulfonamide; iodine; palladium diacetate; silver trifluoroacetate; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; N-ethyl-N,N-diisopropylamine; potassium hexacyanoferrate(III); ruphos; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 2: |Suzuki Coupling / 4: |Sharpless Dihydroxylation;
DOI:10.1021/ol402191t

Reference yield:

: 1450741-59-9
(S,E)-4-(2,6-bis((benzyloxy)methoxy)-4-(prop-1-en-1-yl)phenyl)-3-methylbutan-2-one

: 1450741-64-6
C₃₇H₅₀O₈Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III); potassium osmate; potassium carbonate; methanesulfonamide / water; tert-butyl alcohol / 18 h / 20 °C / Inert atmosphere; Schlenk technique

2: iodine; silver trifluoroacetate / chloroform / 1.5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

3: N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 24 h / 100 °C / 760.05 Torr / Schlenk technique

4: triethylamine; dmap / dichloromethane / 0.25 h / 0 °C / Inert atmosphere; Schlenk technique

With dmap; potassium osmate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; methanesulfonamide; iodine; silver trifluoroacetate; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; N-ethyl-N,N-diisopropylamine; potassium hexacyanoferrate(III); In dichloromethane; chloroform; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1: |Sharpless Dihydroxylation;
DOI:10.1021/ol402191t