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3,5-bis((benzyloxy)methoxy)-4-bromo-1-(E)-prop-1-en-1-ylbenzene

Base Information Edit
  • Chemical Name:3,5-bis((benzyloxy)methoxy)-4-bromo-1-(E)-prop-1-en-1-ylbenzene
  • CAS No.:1450741-55-5
  • Molecular Formula:C25H25BrO4
  • Molecular Weight:469.375
  • Hs Code.:
  • Mol file:1450741-55-5.mol
3,5-bis((benzyloxy)methoxy)-4-bromo-1-(E)-prop-1-en-1-ylbenzene

Synonyms:3,5-bis((benzyloxy)methoxy)-4-bromo-1-(E)-prop-1-en-1-ylbenzene

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Chemical Property of 3,5-bis((benzyloxy)methoxy)-4-bromo-1-(E)-prop-1-en-1-ylbenzene Edit
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Technology Process of 3,5-bis((benzyloxy)methoxy)-4-bromo-1-(E)-prop-1-en-1-ylbenzene

There total 8 articles about 3,5-bis((benzyloxy)methoxy)-4-bromo-1-(E)-prop-1-en-1-ylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); In toluene; for 16h; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1021/ol402191t
Guidance literature:
With 18-crown-6 ether; potassium tert-butylate; In dichloromethane; at 0 - 20 ℃; for 18h; Overall yield = 85 %; Overall yield = 3.74 g; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol402191t
Guidance literature:
Multi-step reaction with 3 steps
1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 0.25 h / -78 - 0 °C / Inert atmosphere; Schlenk technique
2: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex; dimethyl sulfoxide / dichloromethane / 0.25 h / 0 °C / Inert atmosphere; Schlenk technique
3: 18-crown-6 ether; potassium tert-butylate / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
With 18-crown-6 ether; potassium tert-butylate; sulfur trioxide pyridine complex; diisobutylaluminium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; cyclohexane; 3: |Wittig Olefination;
DOI:10.1021/ol402191t
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