(1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methanamine hydrochloride

Base Information

Chemical Name:(1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methanamine hydrochloride
CAS No.:1402585-37-8
Molecular Formula:C₁₁H₈Cl₂F₃N₃*ClH
Molecular Weight:346.567
Hs Code.:

Synonyms:(1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methanamine hydrochloride

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Chemical Property of (1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methanamine hydrochloride

Chemical Property:

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Technology Process of (1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methanamine hydrochloride

There total 5 articles about (1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402585-36-7
1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carbonitrile

: 1402585-37-8
(1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methanamine hydrochloride

Guidance literature:: 1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carbonitrile; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 ℃; for 1h; Reflux;

With hydrogenchloride; In diethyl ether;

Reference yield:

: 13147-14-3
2,3-dichloro-phenylhydrazine

: 1402585-37-8
(1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methanamine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 3 h / Reflux

2: Isovaleronitrile; potassium iodide / acetonitrile / 12 h / Reflux

3: 1-methyl-pyrrolidin-2-one / 2 h / 200 °C

4: dimethylsulfide borane complex / tetrahydrofuran / 1 h / 0 °C / Reflux

With Isovaleronitrile; dimethylsulfide borane complex; potassium iodide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol; acetonitrile;

Reference yield:

: 1402585-35-6
1-(2,3-dichlorophenyl)-5-iodo-3-(trifluoromethyl)-1H-pyrazole

: 1402585-37-8
(1-(2,3-dichlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methanamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1-methyl-pyrrolidin-2-one / 2 h / 200 °C

2: dimethylsulfide borane complex / tetrahydrofuran / 1 h / 0 °C / Reflux

With dimethylsulfide borane complex; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;