[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)]benzylphosphonic acid

Base Information

Chemical Name:[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)]benzylphosphonic acid
CAS No.:852948-48-2
Molecular Formula:C₁₆H₁₇Cl₂O₅P
Molecular Weight:391.188
Hs Code.:

Synonyms:[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)]benzylphosphonic acid

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Chemical Property of [3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)]benzylphosphonic acid

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Technology Process of [3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)]benzylphosphonic acid

There total 5 articles about [3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)]benzylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1056132-78-5
diethyl 3,5-dichloro-4-(4'-hydroxy-3'-iso-propylphenoxy)benzylphosphonate

: 852948-48-2
[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)]benzylphosphonic acid

Guidance literature:: diethyl 3,5-dichloro-4-(4'-hydroxy-3'-iso-propylphenoxy)benzylphosphonate; With trimethylsilyl bromide; In dichloromethane; at -30 - 20 ℃; for 16h;

With boron tribromide; In dichloromethane; at -78 ℃; for 16.1667h;

With water; In dichloromethane; at 0 ℃; Product distribution / selectivity;

Reference yield:

: C₁₇H₁₉Cl₂O₅P

: 852948-48-2
[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)]benzylphosphonic acid

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm800824d

Reference yield:

: 852948-50-6
diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate

: 852948-48-2
[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)]benzylphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl bromide / dichloromethane / 16 h / -30 - 20 °C

2: boron tribromide / dichloromethane / 16.17 h / -78 - 20 °C

With trimethylsilyl bromide; boron tribromide; In dichloromethane;