diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate

Base Information

Chemical Name:diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate
CAS No.:852948-50-6
Molecular Formula:C₂₁H₂₇Cl₂O₅P
Molecular Weight:461.322
Hs Code.:

Synonyms:diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate

Suppliers and Price of diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate

There total 5 articles about diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 852948-49-3
3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzyl bromide

: 122-52-1
triethyl phosphite

: 852948-50-6
diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate

Guidance literature:: In N,N-dimethyl-formamide; at 120 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jm800824d

Reference yield:

: 3337-59-5
methyl 3,5-dichloro-4-hydroxybenzoate

: 852948-50-6
diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: copper; triethylamine / dichloromethane / 72 h / 0 - 20 °C

2: diisobutylaluminium hydride / tetrahydrofuran / 16 h / 0 - 20 °C

3: carbon tetrabromide; triphenylphosphine / diethyl ether / 16 h / 20 °C

4: N,N-dimethyl-formamide / 4 h / Heating / reflux

With carbon tetrabromide; copper; diisobutylaluminium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: bis(3-isopropyl-4-methoxyphenyl)iodonium tetrafluoroborate

: 852948-50-6
diethyl 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)benzylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: copper; triethylamine / dichloromethane / 72 h / 0 - 20 °C

2: diisobutylaluminium hydride / tetrahydrofuran / 16 h / 0 - 20 °C

3: carbon tetrabromide; triphenylphosphine / diethyl ether / 16 h / 20 °C

4: N,N-dimethyl-formamide / 4 h / Heating / reflux

With carbon tetrabromide; copper; diisobutylaluminium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;