N-methylmethoxyphosphinyl-1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine

Base Information

Chemical Name:N-methylmethoxyphosphinyl-1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine
CAS No.:885325-30-4
Molecular Formula:C₂₆H₃₃NO₁₃P₂
Molecular Weight:629.494
Hs Code.:

Synonyms:N-methylmethoxyphosphinyl-1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine

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Chemical Property of N-methylmethoxyphosphinyl-1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine

Chemical Property:

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Technology Process of N-methylmethoxyphosphinyl-1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine

There total 5 articles about N-methylmethoxyphosphinyl-1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine hydrochloride

: 1066-52-0
methyl methylphosphonochloridate

: 885325-30-4
N-methylmethoxyphosphinyl-1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine

Guidance literature:: With triethylamine; In dichloromethane; Heating;
DOI:10.1021/ja0600680

Reference yield:

: Phosphoric acid diphenyl ester (2R,3S,4R,5R)-3,4,6-trihydroxy-5-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-tetrahydro-pyran-2-ylmethyl ester

: 885325-30-4
N-methylmethoxyphosphinyl-1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine

Guidance literature:: Multi-step reaction with 3 steps

1: 15 g / pyridine / 24 h / 20 °C

2: 85 percent / aq. HCl / acetone / Heating

3: 53 percent / Et₃N / CH₂Cl₂ / Heating

With pyridine; hydrogenchloride; triethylamine; In dichloromethane; acetone;
DOI:10.1021/ja0600680

Reference yield:

: 885325-28-0
N-anisylidene 1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine

: 885325-30-4
N-methylmethoxyphosphinyl-1,3,4-tri-O-acetyl-6-diphenylphosphoroglucosamine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / aq. HCl / acetone / Heating

2: 53 percent / Et₃N / CH₂Cl₂ / Heating

With hydrogenchloride; triethylamine; In dichloromethane; acetone;
DOI:10.1021/ja0600680