C₁₂H₁₅NO₃

Base Information

Chemical Name:C₁₂H₁₅NO₃
CAS No.:1315331-70-4
Molecular Formula:C₁₂H₁₅NO₃
Molecular Weight:221.256
Hs Code.:

C<sub>12</sub>H<sub>15</sub>NO<sub>3</sub>

Synonyms:C₁₂H₁₅NO₃

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Chemical Property of C₁₂H₁₅NO₃

Chemical Property:

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Technology Process of C₁₂H₁₅NO₃

There total 3 articles about C₁₂H₁₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1315331-68-0
C₁₆H₂₃NO₄S

: 1315331-70-4
C₁₂H₁₅NO₃

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; optical yield given as %ee; Inert atmosphere;
DOI:10.1002/ejoc.201100352

Reference yield:

: 1315331-65-7
C₁₈H₂₇NO₅S

: 1315331-70-4
C₁₂H₁₅NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; benzyl bromide / methanol / 1 h / 0 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; benzyl bromide; In 1,4-dioxane; methanol;
DOI:10.1002/ejoc.201100352

Reference yield:

: 30277-63-5
3-methoxy-3-(4-methoxyphenyl)propene

: 1315331-70-4
C₁₂H₁₅NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; lithium triethylborohydride; magnesium bromide / tetrahydrofuran / -50 - 20 °C / Inert atmosphere

2: sodium tetrahydroborate; benzyl bromide / methanol / 1 h / 0 °C / Inert atmosphere

3: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; benzyl bromide; lithium triethylborohydride; magnesium bromide; In tetrahydrofuran; 1,4-dioxane; methanol; 1: Mannich reaction;
DOI:10.1002/ejoc.201100352