4-[3-(3,4,6,7,12,12a-Hexahydro-1H-pyrazino[1',2':1,6]pyrido[3,4-b]indol-2-yl)-propane-1-sulfonyl]-phenylamine

Base Information

Chemical Name:4-[3-(3,4,6,7,12,12a-Hexahydro-1H-pyrazino[1',2':1,6]pyrido[3,4-b]indol-2-yl)-propane-1-sulfonyl]-phenylamine
CAS No.:115041-62-8
Molecular Formula:C₂₃H₂₈N₄O₂S
Molecular Weight:424.567
Hs Code.:

Synonyms:4-[3-(3,4,6,7,12,12a-Hexahydro-1H-pyrazino[1',2':1,6]pyrido[3,4-b]indol-2-yl)-propane-1-sulfonyl]-phenylamine

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Chemical Property of 4-[3-(3,4,6,7,12,12a-Hexahydro-1H-pyrazino[1',2':1,6]pyrido[3,4-b]indol-2-yl)-propane-1-sulfonyl]-phenylamine

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Technology Process of 4-[3-(3,4,6,7,12,12a-Hexahydro-1H-pyrazino[1',2':1,6]pyrido[3,4-b]indol-2-yl)-propane-1-sulfonyl]-phenylamine

There total 4 articles about 4-[3-(3,4,6,7,12,12a-Hexahydro-1H-pyrazino[1',2':1,6]pyrido[3,4-b]indol-2-yl)-propane-1-sulfonyl]-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 115041-61-7
γ-chloropropyl 4-aminophenyl sulphone

: 55344-28-0
1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4-b>indole

: 115041-62-8
4-[3-(3,4,6,7,12,12a-Hexahydro-1H-pyrazino[1',2':1,6]pyrido[3,4-b]indol-2-yl)-propane-1-sulfonyl]-phenylamine

Guidance literature:: With sodium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 80 ℃;

Reference yield:

: 78234-11-4
γ-chloropropyl-4-acetamidophenyl sulphide

: 115041-62-8
4-[3-(3,4,6,7,12,12a-Hexahydro-1H-pyrazino[1',2':1,6]pyrido[3,4-b]indol-2-yl)-propane-1-sulfonyl]-phenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 1) KMnO₄, 2) H₂O₂ / aq. acetic acid / 1) 30 deg C, 4 h

2: 55 percent / 18percent HCl / 130 °C

3: 48 percent / NaI, Na₂CO₃ / dimethylformamide / 80 °C

With hydrogenchloride; potassium permanganate; dihydrogen peroxide; sodium carbonate; sodium iodide; In acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 78234-18-1
γ-chloropropyl 4-acetamidophenyl sulphone

: 115041-62-8
4-[3-(3,4,6,7,12,12a-Hexahydro-1H-pyrazino[1',2':1,6]pyrido[3,4-b]indol-2-yl)-propane-1-sulfonyl]-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / 18percent HCl / 130 °C

2: 48 percent / NaI, Na₂CO₃ / dimethylformamide / 80 °C

With hydrogenchloride; sodium carbonate; sodium iodide; In N,N-dimethyl-formamide;