O-(2,3-di-O-para-methoxybenzyl-α-D-galactopyranosyl)-N-dodecanoyl-L-serine undecylamide

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Chemical Name:O-(2,3-di-O-para-methoxybenzyl-α-D-galactopyranosyl)-N-dodecanoyl-L-serine undecylamide
CAS No.:1293922-60-7
Molecular Formula:C₄₈H₇₈N₂O₁₀
Molecular Weight:843.155
Hs Code.:

Synonyms:O-(2,3-di-O-para-methoxybenzyl-α-D-galactopyranosyl)-N-dodecanoyl-L-serine undecylamide

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Chemical Property of O-(2,3-di-O-para-methoxybenzyl-α-D-galactopyranosyl)-N-dodecanoyl-L-serine undecylamide

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Technology Process of O-(2,3-di-O-para-methoxybenzyl-α-D-galactopyranosyl)-N-dodecanoyl-L-serine undecylamide

There total 6 articles about O-(2,3-di-O-para-methoxybenzyl-α-D-galactopyranosyl)-N-dodecanoyl-L-serine undecylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1293922-59-4
O-(2,3-di-O-para-methoxybenzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-N-dodecanoyl-L-serine undecylamide

: 1293922-60-7
O-(2,3-di-O-para-methoxybenzyl-α-D-galactopyranosyl)-N-dodecanoyl-L-serine undecylamide

Guidance literature:: With vanadyl triflate; In methanol; dichloromethane; acetonitrile; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1039/c0ob00990c

Reference yield:

: 1293922-41-4
4-methylphenyl 4,6-0-benzylidene-2,3-di-0-(4-methoxybenzyl)-1-thio-β-D-galactopyranoside

: 1293922-60-7
O-(2,3-di-O-para-methoxybenzyl-α-D-galactopyranosyl)-N-dodecanoyl-L-serine undecylamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

2.1: 4-methyl-morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.1: piperidine / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

6.1: vanadyl triflate / methanol; dichloromethane; acetonitrile / 6 h / 20 °C / Inert atmosphere

With piperidine; 4-methyl-morpholine; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; vanadyl triflate; trifluorormethanesulfonic acid; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1039/c0ob00990c

Reference yield:

: 1293922-47-0
N-(9-fluorenylmethoxycarbonyl)-O-(2,3-di-O-para-methoxybenzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-L-serine allyl ester

: 1293922-60-7
O-(2,3-di-O-para-methoxybenzyl-α-D-galactopyranosyl)-N-dodecanoyl-L-serine undecylamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: 4-methyl-morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.1: piperidine / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

5.1: vanadyl triflate / methanol; dichloromethane; acetonitrile / 6 h / 20 °C / Inert atmosphere

With piperidine; 4-methyl-morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; vanadyl triflate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1039/c0ob00990c