4-Methylphenyl 4,6-O-Benzylidene-2,3-di-O-(4-methoxybenzyl)--D-thiogalactopyranoside

Base Information

Chemical Name:4-Methylphenyl 4,6-O-Benzylidene-2,3-di-O-(4-methoxybenzyl)--D-thiogalactopyranoside
CAS No.:1293922-41-4
Molecular Formula:C₃₆H₃₈O₇S
Molecular Weight:614.76
Hs Code.:
Mol file:1293922-41-4.mol

Synonyms:4-methylphenyl 4,6-0-benzylidene-2,3-di-0-(4-methoxybenzyl)-1-thio-β-D-galactopyranoside

Suppliers and Price of 4-Methylphenyl 4,6-O-Benzylidene-2,3-di-O-(4-methoxybenzyl)--D-thiogalactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Methylphenyl4,6-O-Benzylidene-2,3-di-O-(4-methoxybenzyl)-β-D-thiogalactopyranoside
1g
$ 165.00

American Custom Chemicals Corporation
4-METHYLPHENYL-4,6-O-BENZYLIDENE-2,3-DI-O-(4-METHOXYBENZYL)-BETA-D-THIOGALACTOPYRANOSIDE 95.00%
5MG
$ 495.30

Total 4 raw suppliers

Chemical Property of 4-Methylphenyl 4,6-O-Benzylidene-2,3-di-O-(4-methoxybenzyl)--D-thiogalactopyranoside

Chemical Property:

Melting Point:127-129°C
Boiling Point:731.8±60.0 °C(Predicted)
Density:1.27±0.1 g/cm3(Predicted)
Solubility.:Chloroform, Dichloromethane, DMF, DMSO, Ethyl Acetate, Methanol

Purity/Quality:

98%min ^*data from raw suppliers

4-Methylphenyl4,6-O-Benzylidene-2,3-di-O-(4-methoxybenzyl)-β-D-thiogalactopyranoside ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 4-Methylphenyl 4,6-O-Benzylidene-2,3-di-O-(4-methoxybenzyl)-β-D-thiogalactopyranoside (cas# 1293922-41-4) is a compound useful in organic synthesis.

Technology Process of 4-Methylphenyl 4,6-O-Benzylidene-2,3-di-O-(4-methoxybenzyl)--D-thiogalactopyranoside

There total 1 articles about 4-Methylphenyl 4,6-O-Benzylidene-2,3-di-O-(4-methoxybenzyl)--D-thiogalactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 824-94-2
p-methoxybenzyl chloride

: 161007-96-1
(p-methylphenyl) 4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 1293922-41-4
4-methylphenyl 4,6-0-benzylidene-2,3-di-0-(4-methoxybenzyl)-1-thio-β-D-galactopyranoside

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 65 - 70 ℃; for 1h;

Reference yield: 96.0%

: 1293922-41-4
4-methylphenyl 4,6-0-benzylidene-2,3-di-0-(4-methoxybenzyl)-1-thio-β-D-galactopyranoside

: 4,6-O-benzylidene-2,3-di-O-(4-methoxybenzyl)-α,β-D-galactopyranoside

Guidance literature:: 4-methylphenyl 4,6-0-benzylidene-2,3-di-0-(4-methoxybenzyl)-1-thio-β-D-galactopyranoside; With N-Bromosuccinimide; In acetone; at -20 ℃; for 0.75h;

With water; sodium hydrogencarbonate; In acetone;

Reference yield: 63.0%

: 1293922-41-4
4-methylphenyl 4,6-0-benzylidene-2,3-di-0-(4-methoxybenzyl)-1-thio-β-D-galactopyranoside

: 136497-85-3
N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester

: 1293922-47-0
N-(9-fluorenylmethoxycarbonyl)-O-(2,3-di-O-para-methoxybenzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-L-serine allyl ester

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;
DOI:10.1039/c0ob00990c