N,N'-Dichloro-3-phenylpentandiamid

Base Information

• Chemical Name: N,N'-Dichloro-3-phenylpentandiamid
• CAS No.: 84557-85-7
• Molecular Formula: C₁₁H₁₂Cl₂N₂O₂
• Molecular Weight: 275.134
• Mol file: 84557-85-7.mol

Synonyms:N,N'-Dichloro-3-phenylpentandiamid

Chemical Property of N,N'-Dichloro-3-phenylpentandiamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-Dichloro-3-phenylpentandiamid

There total 2 articles about N,N'-Dichloro-3-phenylpentandiamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-Phenylpentandiamid (78533-83-2) → N,N'-Dichloro-3-phenylpentandiamid (84557-85-7)

Guidance literature:

With chlorine; In hydrogenchloride; at 5 ℃; for 3h;

DOI:10.1055/s-1982-30030

Reference yield:

diethyl 3-phenylpentanedioate (55951-74-1) → N,N'-Dichloro-3-phenylpentandiamid (84557-85-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / ammonia / 5 h / 110 °C

2: 80 percent / chlorine / aq. HCl / 3 h / 5 °C

With ammonia; chlorine; In hydrogenchloride;

DOI:10.1055/s-1982-30030

Reference yield: 17.0%

N,N'-Dichloro-3-phenylpentandiamid (84557-85-7) → 2,4-Dioxo-6-phenylhexahydro-1,3-diazepin (84557-82-4)

Guidance literature:

With triethylamine; In 1,4-dioxane; at 60 ℃; for 1h;

DOI:10.1055/s-1982-30030

upstream raw materials:

3-Phenylpentandiamid

diethyl 3-phenylpentanedioate

Downstream raw materials:

2,4-Dioxo-6-phenylhexahydro-1,3-diazepin