Technology Process of C22H19NO7
There total 5 articles about C22H19NO7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C29H25NO7;
With
water; potassium hydroxide;
In
tetrahydrofuran;
at 20 ℃;
With
hydrogenchloride;
In
water;
pH=2;
Cooling in ice;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / acetonitrile / Reflux
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C
3.1: potassium hydroxide; water / tetrahydrofuran / 80 °C
3.2: pH 2 / Cooling in ice
4.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C
5.1: potassium hydroxide; water / tetrahydrofuran / 20 °C
5.2: pH 2 / Cooling in ice
With
water; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C
2.1: potassium hydroxide; water / tetrahydrofuran / 80 °C
2.2: pH 2 / Cooling in ice
3.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C
4.1: potassium hydroxide; water / tetrahydrofuran / 20 °C
4.2: pH 2 / Cooling in ice
With
water; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;