benzyl 3,4,6-tri-O-benzyl-2-[(tert-butoxycarbonyl)amino]-2-deoxy-D-glucopyranoside

Base Information

Chemical Name:benzyl 3,4,6-tri-O-benzyl-2-[(tert-butoxycarbonyl)amino]-2-deoxy-D-glucopyranoside
CAS No.:1281971-23-0
Molecular Formula:C₃₉H₄₅NO₇
Molecular Weight:639.789
Hs Code.:

Synonyms:benzyl 3,4,6-tri-O-benzyl-2-[(tert-butoxycarbonyl)amino]-2-deoxy-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3,4,6-tri-O-benzyl-2-[(tert-butoxycarbonyl)amino]-2-deoxy-D-glucopyranoside

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Technology Process of benzyl 3,4,6-tri-O-benzyl-2-[(tert-butoxycarbonyl)amino]-2-deoxy-D-glucopyranoside

There total 4 articles about benzyl 3,4,6-tri-O-benzyl-2-[(tert-butoxycarbonyl)amino]-2-deoxy-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2-deoxy-2<<(1,1-dimethylethoxy)carbonyl>amino>-D-glucopyranose

: 100-39-0
benzyl bromide

: 1281971-23-0
benzyl 3,4,6-tri-O-benzyl-2-[(tert-butoxycarbonyl)amino]-2-deoxy-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;
DOI:10.1021/jo1023156

Reference yield:

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 1281971-23-0
benzyl 3,4,6-tri-O-benzyl-2-[(tert-butoxycarbonyl)amino]-2-deoxy-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: water; triethylamine / ethanol

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

With water; sodium hydride; triethylamine; In ethanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo1023156

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1281971-23-0
benzyl 3,4,6-tri-O-benzyl-2-[(tert-butoxycarbonyl)amino]-2-deoxy-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: water; triethylamine / ethanol

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

With water; sodium hydride; triethylamine; In ethanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo1023156