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Technology Process of (PtH(C10H6(CN(CH3)2C6H3)2)(CH2CH2))(1+)*(((CF3)2C6H3)4B)(1-)=(PtH(C10H6(CN(CH3)2C6H3)2)(C2H4))(((CF3)2C6H3)4B)

(PtH(C10H6(CN(CH3)2C6H3)2)(CH2CH2))(1+)*(((CF3)2C6H3)4B)(1-)=(PtH(C10H6(CN(CH3)2C6H3)2)(C2H4))(((CF3)2C6H3)4B)

Base Information
  • Chemical Name:(PtH(C10H6(CN(CH3)2C6H3)2)(CH2CH2))(1+)*(((CF3)2C6H3)4B)(1-)=(PtH(C10H6(CN(CH3)2C6H3)2)(C2H4))(((CF3)2C6H3)4B)
  • CAS No.:932013-17-7
  • Molecular Formula:C30H29N2Pt*C32H12BF24
  • Molecular Weight:1475.87
  • Hs Code.:
(PtH(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(CH<sub>2</sub>CH<sub>2</sub>))<sup>(1+)</sup>*(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)<sup>(1-)</sup>=(PtH(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(C<sub>2</sub>H<sub>4</sub>))(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)

Synonyms:(PtH(C10H6(CN(CH3)2C6H3)2)(CH2CH2))(1+)*(((CF3)2C6H3)4B)(1-)=(PtH(C10H6(CN(CH3)2C6H3)2)(C2H4))(((CF3)2C6H3)4B)

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Chemical Property of (PtH(C10H6(CN(CH3)2C6H3)2)(CH2CH2))(1+)*(((CF3)2C6H3)4B)(1-)=(PtH(C10H6(CN(CH3)2C6H3)2)(C2H4))(((CF3)2C6H3)4B)
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Technology Process of (PtH(C10H6(CN(CH3)2C6H3)2)(CH2CH2))(1+)*(((CF3)2C6H3)4B)(1-)=(PtH(C10H6(CN(CH3)2C6H3)2)(C2H4))(((CF3)2C6H3)4B)

There total 2 articles about (PtH(C10H6(CN(CH3)2C6H3)2)(CH2CH2))(1+)*(((CF3)2C6H3)4B)(1-)=(PtH(C10H6(CN(CH3)2C6H3)2)(C2H4))(((CF3)2C6H3)4B) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

Brookhart's acid

Brookhart's acid

Pt(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(CH<sub>2</sub>CH<sub>3</sub>)2
932013-22-4

Pt(C10H6(CN(CH3)2C6H3)2)(CH2CH3)2

(PtH(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(CH<sub>2</sub>CH<sub>2</sub>))<sup>(1+)</sup>*(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)<sup>(1-)</sup>=(PtH(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(C<sub>2</sub>H<sub>4</sub>))(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)
932013-17-7

(PtH(C10H6(CN(CH3)2C6H3)2)(CH2CH2))(1+)*(((CF3)2C6H3)4B)(1-)=(PtH(C10H6(CN(CH3)2C6H3)2)(C2H4))(((CF3)2C6H3)4B)

Guidance literature:
In diethyl ether; under N2 atm. soln. (H(OEt2)2)(BAr4) in Et2O was cooled to -78°C and added dropwise to soln. Pt complex in Et2O at -78°C, mixt. was placed under vac. at -78°C for 4.5 h, warmed to room temp.; mixt. was evapd. in vac., residue was recrystd. from CH2Cl2/pentane, filtered, dried in vac.; elem. anal.;
DOI:10.1021/ja068118o

Reference yield:

ethene
74-85-1

ethene

(PtH(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(CH<sub>3</sub>CH<sub>2</sub>C<sub>2</sub>H<sub>3</sub>))<sup>(1+)</sup>*(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)<sup>(1-)</sup>=(Pt(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(CH<sub>3</sub>CH<sub>2</sub>C<sub>2</sub>H<sub>3</sub>H))(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)
932013-21-3

(PtH(C10H6(CN(CH3)2C6H3)2)(CH3CH2C2H3))(1+)*(((CF3)2C6H3)4B)(1-)=(Pt(C10H6(CN(CH3)2C6H3)2)(CH3CH2C2H3H))(((CF3)2C6H3)4B)

(PtH(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(CH<sub>2</sub>CH<sub>2</sub>))<sup>(1+)</sup>*(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)<sup>(1-)</sup>=(PtH(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(C<sub>2</sub>H<sub>4</sub>))(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)
932013-17-7

(PtH(C10H6(CN(CH3)2C6H3)2)(CH2CH2))(1+)*(((CF3)2C6H3)4B)(1-)=(PtH(C10H6(CN(CH3)2C6H3)2)(C2H4))(((CF3)2C6H3)4B)

Guidance literature:
In dichloromethane-d2; react. Pt complex with excess ethylene in CD2Cl2 at -78 ° C; monitoring by NMR spectroscopy; Kinetics;
DOI:10.1021/ja068118o

Reference yield: 88.0%

ethene
74-85-1

ethene

(PtH(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(CH<sub>2</sub>CH<sub>2</sub>))<sup>(1+)</sup>*(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)<sup>(1-)</sup>=(PtH(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(C<sub>2</sub>H<sub>4</sub>))(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)
932013-17-7

(PtH(C10H6(CN(CH3)2C6H3)2)(CH2CH2))(1+)*(((CF3)2C6H3)4B)(1-)=(PtH(C10H6(CN(CH3)2C6H3)2)(C2H4))(((CF3)2C6H3)4B)

(Pt(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(CH<sub>2</sub>CH<sub>2</sub>)(C<sub>2</sub>H<sub>5</sub>))<sup>(1+)</sup>*(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)<sup>(1-)</sup>=(Pt(C<sub>10</sub>H<sub>6</sub>(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2)(C<sub>2</sub>H<sub>4</sub>)(C<sub>2</sub>H<sub>5</sub>))(((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4B)
932013-19-9

(Pt(C10H6(CN(CH3)2C6H3)2)(CH2CH2)(C2H5))(1+)*(((CF3)2C6H3)4B)(1-)=(Pt(C10H6(CN(CH3)2C6H3)2)(C2H4)(C2H5))(((CF3)2C6H3)4B)

Guidance literature:
In dichloromethane; soln. Pt complex in CH2Cl2 at 0°C was purged with ethylene for 5 min; pentane was added, ppt. was collected by filtration, dried under vac.; elem. anal.;
DOI:10.1021/ja068118o
upstream raw materials:

ethene

(PtH(C10H6(CN(CH3)2C6H3)2)(CH3CH2C2H3))(1+)*(((CF3)2C6H3)4B)(1-)=(Pt(C10H6(CN(CH3)2C6H3)2)(CH3CH2C2H3H))(((CF3)2C6H3)4B)

Pt(C10H6(CN(CH3)2C6H3)2)(CH2CH3)2

Downstream raw materials:

(Pt(C10H6(CN(CH3)2C6H3)2)(CH2CH2)(C2H5))(1+)*(((CF3)2C6H3)4B)(1-)=(Pt(C10H6(CN(CH3)2C6H3)2)(C2H4)(C2H5))(((CF3)2C6H3)4B)

(PtH(C10H6(CN(CH3)2C6H3)2)(CH3CH2C2H3))(1+)*(((CF3)2C6H3)4B)(1-)=(Pt(C10H6(CN(CH3)2C6H3)2)(CH3CH2C2H3H))(((CF3)2C6H3)4B)

Pt(C10H6(CN(CH3)2C6H3)2)(CH3CH2)(CH3CN)(1+)*(((CF3)2C6H3)4B)(1-)=(Pt(C10H6(CN(CH3)2C6H3)2)(C2H5)(CH3CN))(((CF3)2C6H3)4B)

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