Technology Process of 1-fluoro-2,2-diphenyl-1-phenylsulfonylcyclopropane
There total 4 articles about 1-fluoro-2,2-diphenyl-1-phenylsulfonylcyclopropane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform;
at -20 - 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1246/cl.130570
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Selectfluor / acetonitrile / 0.42 h / 0 - 20 °C / Inert atmosphere
2: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / dichloromethane; water / 9 h / 45 °C
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane; chloroform / 7 h / -20 - 20 °C
4: 3-chloro-benzenecarboperoxoic acid / chloroform / 16 h / -20 - 20 °C / Inert atmosphere
With
N-benzyl-N,N,N-triethylammonium chloride; Selectfluor; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide;
In
dichloromethane; chloroform; water; acetonitrile;
DOI:10.1246/cl.130570
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; chloroform / 7 h / -20 - 20 °C
2: 3-chloro-benzenecarboperoxoic acid / chloroform / 16 h / -20 - 20 °C / Inert atmosphere
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; chloroform;
DOI:10.1246/cl.130570
