1-hydroxy-1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid lactone

Base Information

Chemical Name:1-hydroxy-1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid lactone
CAS No.:135107-76-5
Molecular Formula:C₂₀H₂₀O₃
Molecular Weight:308.377
Hs Code.:

Synonyms:1-hydroxy-1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid lactone

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Chemical Property of 1-hydroxy-1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid lactone

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Technology Process of 1-hydroxy-1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid lactone

There total 4 articles about 1-hydroxy-1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6742-31-0
1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid

: 135107-76-5
1-hydroxy-1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / conc. H₂SO₄ / benzene / 24 h / Heating

With sulfuric acid; In benzene;
DOI:10.1021/jo00018a030

Reference yield:

: 6627-55-0
2-bromo-p-cresol

: 135107-76-5
1-hydroxy-1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / NaOH / H₂O / 2 h / Heating

With sodium hydroxide; In water;
DOI:10.1021/jo00018a030

Reference yield:

: 1-(2-Methoxycarbonylmethyl-3,4-dihydro-2H-naphthalen-1-ylidene)-pyrrolidinium; bromide

: 135107-76-5
1-hydroxy-1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid lactone

Guidance literature:: Multi-step reaction with 2 steps

1: water / methanol / 0.5 h / steam bath

With water; In methanol;
DOI:10.1021/jo00018a030