trans 1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid methyl ester

Base Information

Chemical Name:trans 1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid methyl ester
CAS No.:135107-80-1
Molecular Formula:C₂₁H₂₄O₃
Molecular Weight:324.42
Hs Code.:

Synonyms:trans 1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid methyl ester

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Chemical Property of trans 1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid methyl ester

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Technology Process of trans 1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid methyl ester

There total 7 articles about trans 1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6742-31-0
1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid

: 135107-80-1
trans 1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / conc. H₂SO₄ / benzene / 24 h / Heating

3: H₂ / 10percent Pd-C / acetic acid / 5 h / 65 - 68 °C

4: tetrahydrofuran

With sulfuric acid; hydrogen; palladium on activated charcoal; In tetrahydrofuran; acetic acid; benzene;
DOI:10.1021/jo00018a030

Reference yield:

: 6627-55-0
2-bromo-p-cresol

: 135107-80-1
trans 1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / NaOH / H₂O / 2 h / Heating

3: H₂ / 10percent Pd-C / acetic acid / 5 h / 65 - 68 °C

4: tetrahydrofuran

With sodium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; water; acetic acid;
DOI:10.1021/jo00018a030

Reference yield:

: 22002-45-5
2-bromo-4-methylanisole

: 135107-80-1
trans 1-(2'-methoxy-5'-methylphenyl)-1,2,3,4-tetrahydro-2-naphthaleneacetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: H₂ / 10percent Pd-C / acetic acid / 5 h / 65 - 68 °C

3: tetrahydrofuran

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; acetic acid;
DOI:10.1021/jo00018a030